البحث — المستودع الرقمي العراقي

نتائج البحث: 15 من أصل 90

الدراسة العملية وتحليل دايناميك الموائع المتحركه لنظام الطبقة المتميعه == EXPERIMENTAL STUDY AND COMPUTATIONAL FLUID DYNAMIC SIMULATION of CIRCULATING FLUIDIZED BED

اسم المؤلف: حنين ثامر شطب

اسم المشرف: سعد ناهي صالح | احمد عبد محمد

الموضوع العام: الهندسة الكيمياوية

السنة: 2016

الموضوع الدقيق: الهندسة الكيمياوية

الدرجة: ماجستير

الجامعة: جامعة تكريت - كلية الهندسة - قسم الهندسة الكيمياوية

اللغة: الانكليزية

مكان الجامعة: صلاح الدين

الصفحات الاولى:

دراسة تاثير بعض متغيرات عملية الترسيب الكهروكيمياوي للنحاس على كفاءة العملية وخواص المسحوق المنتج == The Study of The Effect of Some Variables in Electrochemical Deposition of Copper Powder on The Efficiency of Process And Powder Properties

اسم المؤلف: ميادة نوار نصيف

اسم المشرف: فاروق منصور مهدي

الموضوع العام: الهندسة الكيمياوية

السنة: 2010

الموضوع الدقيق: الهندسة الكيمياوية

الدرجة: ماجستير

الجامعة: جامعة تكريت - كلية الهندسة - قسم الهندسة الكيمياوية

اللغة: الانكليزية

مكان الجامعة: صلاح الدين

الصفحات الاولى:

المستخلص: يهدف البحث الى اجراء دراسة عملية لانتاج مسحوق النحاس باستعمال طريقة الترسيب الكهروكيمياوية مع دراسة تاثير عدد من المتغيرات التي تؤثر في كفاءة العملية والوقوف على طبيعة تاثير كل منها. تمت دراسة تاثير كل من كثافة التيار وزمن الترسيب ودرجة حرارة وسط الترسيب | The present study aims to produce copper powder by the electrochemical deposition method. In this work, the effect of current density, deposition period, electrolyte temperature, distance between electrodes, ratio of anode to cathode surface area and cathode rotation on the current efficiency and powder properties such as apparent density, grain size, grain size distribution and grain morphology on powder properties and current efficiency are studied. A deposition system composed of Perspex cell, two copper electrodes ( 96.8% purity), electrolyte composed of 90g/l CuSO4 and 120g/l H2SO4 as well as the electrical connections. Betts method was followed by this study.The automatic sieve shaker was used to determine the grain size, while the atomic spectroscopy was used to determine copper purity. Moreover, both optical microscope and SEM were used to estimate powder morphology. It is found that current efficiency is increased with increasing deposition time and electrolyte temperature. It is also found to be decreased with increasing current density, distance between the electrodes, ratio of anode to cathode surface area and rotation of cathode electrode. The results showed also that particle size is increased with increasing the distance between the electrodes and increased with increasing the ratio of anode to cathode surface area and cathode rotation. Further more, the obtained data indicated that the maximum and minimum achieved fine grain percent (

اكسدة ايون الحديدوز الى ايون الحديديك باستخدام المضافات في العمود ذو الفقاعة == Oxidation of Ferrous To Ferric Ion By Additives in Bubble Column

اسم المؤلف: صباح محمد حسن الجبوري

اسم المشرف: رافع جمال يعقوب

الموضوع العام: الهندسة الكيمياوية

السنة: 2014

الموضوع الدقيق: الهندسة الكيمياوية

الدرجة: ماجستير

الجامعة: جامعة تكريت - كلية الهندسة - قسم الهندسة الكيمياوية

اللغة: الانكليزية

مكان الجامعة: صلاح الدين

الصفحات الاولى:

المستخلص: تم دراسة اكسدة كبريتات الحديدوز الى كبريتات الحديديك من خلال التركيز على اختبار تاثير الظروف التشغيلية للمنظومة على عملية اكسدة كبريتات الحديدوز بالهواء ومن ثم دراسة تاثير المضافات في اتمام عملية الاكسدة باستخدام الاوكسجين في العمود الفقاعي. تم استخدام ا | This study was discussion converting of ferrous sulfate to ferric sulfate by oxidation with using the bubble column and concentrates by using air and then studied the effect of additives to complete the oxidation with oxygen. Air is used as an oxidation agent in the first step to study the oxidation reaction in bubble column with(5 cm inside diameter ,120 cm tall ), in this part of process, studying the operation condition on the oxidation and determining the rate of conversion. Temperature ( 50,60 and 70 )°C ,air flow rate (100,150,200 and 250)L/h and initial concentration of ferrous (0.5 , 0.25 , 0.1 and 0.05 )M with fixing the pressure slightly up to 1 atmosphere are used to study the performance of the parameters (initial concentration ,temperature and air flow rate on oxidation ferrous sulfate.The effect of these conditions are studied throughout the experimental work to increase the conversion rate of ferrous sulfate.The results are shown that the maximum conversion rate is 53.5% at the temperature 70 °C ,air flow rate 150 L/h and initial concentration of ferrous is 0.1M.The results of the optimum conditions are depended on the second part of this work by using oxygen gas and additive material, (CuSO4, KMnO4, H2O2 and HNO3) at the different concentration (100 , 200 , 300 , 400 , 500 ) ppm, the effect of each material is studied to show the conversion rate of ferrous to ferric sulfate.The test of these material gave different results for each material and gave different result for each concentration of additive on the conversion rate of ferrous.The best result is that the conversion rate is 81.1 % by using CuSO4 at additive concentration 400ppm, the conversion rate is 78.9% by using HNO3 at concentration of additive 200 ppm , the conversion rate is 73.1% by using KMnO4 at concentration of additive 400 ppm and the conversion rate is 70% by using H2O2 at concentration of additive 200 ppm.Mathematical correlation for each additive and the main operating variables on oxidation of ferrous to ferric sulfate are solved by using (Excel) program are illustrated : - (d[?Fe?^(+2)])/dt=0.612067 t+0.011378 Cadd ? 2.86622.

تاثير المحتوى المائي، درجة الحرارة وكلوريد الصوديوم على تاكل CO2 للصلب الكربوني (A106 B) في النفط العراقي == Effect of Water Content , Temperature And NaCl on CO2 Corrosion of C - Steel (A 106 B) in Iraqi Crude Oil

اسم المؤلف: انعام يوسف عبد الرحمن

اسم المشرف: سعد احمد جعفر

الموضوع العام: الهندسة الكيمياوية

السنة: 2014

الموضوع الدقيق: الهندسة الكيمياوية

الدرجة: ماجستير

الجامعة: جامعة تكريت - كلية الهندسة - قسم الهندسة الكيمياوية

اللغة: الانكليزية

مكان الجامعة: صلاح الدين

الصفحات الاولى:

المستخلص: ان التاكل الداخلي في انابيب الصلب الكربوني الذي يحدث بوجود غاز ثاني اوكسيد الكربون يعتبر مشكلة جوهرية في صناعات النفط والغاز وهو يقترن دائما مع وجود الماء. ان احتمالية حدوث التاكل تزداد بصورة عامة مع تزايد نسبة الماء ومع زيادة مستوى الماء المنتج تزداد مع | Internal corrosion of carbon steel pipelines occurring in the presence of CO2 is a substantial problem in the oil and gas industries. It is always associated with the presence of free water. The likelihood of corrosion generally increases with the volume fraction of the water phase. As the produced water level increases, the corrosion rates of carbon steel increase very rapidly and causes damage of petroleum and gas pipelines. The present research work focuses on the investigating of the corrosion rate of carbon steel as flow line in crude oil production with CO2 content employing three Iraqi crude oil (Kirkuk crude oil, Halfaya crude oil, Rumalia crude oil) with different brine concentrations [1%NaCl, 2%NaCl, 3%NaCl]. Determining the corrosivity of Iraqi crude oil was studied for the first time. Experiments were performed in an autoclave test apparatus, crude oil - produced water mixtures, water cuts were (0, 10, 20, 30, 40, and 100%), and total volume of mixtures inside the autoclave was always kept at 100ml and temperature (20, 40, 60°C). For all experiments, CO2 partial pressure was maintained at (4 bar) and rotational speed (500 rpm).The corrosion rates were determined by the weight loss technique. The results revealed that the corrosion rates of carbon steel increased by increasing water cut and temperature, but decreases with increasing salt concentration for all types of crude oil. Results also indicated that different crude oil has significantly different effects on corrosion of carbon steel, with identical brine compositions. Therefore, Rumaila crude oil exhibits the highest corrosion rates and Kirkuk crude oil exhibits the lowest corrosion rates while Halfaya crude oil exhibits a moderate corrosion rates e.g. at 1% NaCl, 20% water cut, temperature 60°C, pressure 4bar, the corrosion rate of carbon steel in Rumaila crude oil is 0.9163mm/yr whereas it is 0.564 mm/yr and 0.705 mm/yr in Kirkuk crude oil and Halfaya crude oil respectively. The Corrosion Rate Break produced water level was determined from the experiments. These tests are employed to evaluate the requirements for corrosion inhibitor treatment. At 100% water cut (brine/CO2) the corrosion rates of carbon steel was the highest. The presence of crude oil decreases the corrosion rates e.g. at 1% NaCl,100% water cut(brine/CO2) the corrosion rate is 7.1197 mm/yr, whereas at 40% water cut/ Rumaila crude oil the corrosion rate is 1.4097 mm/yr.