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اللحام النقطي بالاحتكاك و الخلط لسبيكة الالمنيوم 3105 == Friction Stir spot Welding of Aluminum Alloy 3105

Author name: فالح حسين صدام
Supervisor name: احمد عودة جاسم
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: English
University location: Babylon
First pages:

تاثير اللحام بالتنكستن TIG وبالقوس الكهربائي (SMAW) على البنيه المجهرية والخواص الميكانيكية للفولاذ واطئ الكربون == Effect of TIG and SMAW welding parameters on the microstructure and mechanical properties of low carbon steel

Author name: علي جاسم عطية لفته
Supervisor name: اقبال محمد سعيد صالح
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: Arabic
University location: Babylon
First pages:

التحقق من الخواص الميكانيكية لوصلة لحام لانبوب المراجل البخارية في محطات توليد الطاقة == Investigation of the Mechanical properties of the tube boiler weld joint in the Power plants

Author name: محمد عبد الرضا كاظم الزبيدي
Supervisor name: كاظم فنطيل السلطاني
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: Arabic
University location: Babylon
First pages:

تاثير اضافة عنصر الفضة على بعض الخواص الميكانيكية لسبائك البراص == Effect of Silver Addition on Some Mechanical Properties of Brass Alloys

Author name: ايمان سليمان عبيد
Supervisor name: علي هوبي حليم
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: English
University location: Babylon
First pages:

دور السباكة تحت تاثير الاهتزاز والتعتيق اللاحق على الخواص الميكانيكية لسبيكة Al - 4%Cu == The Role of casting under vibration and Subsequent Aging on Mechanical Properties of Al - 4%Cu

Author name: رانية حسين ياسين الخفاجي
Supervisor name: حيدر العذاري
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: English
University location: Babylon
First pages:

دراسة بعض الخواص الميكانيكية لسبيكة المنيوم % 4 نحاس معصورة == Study of Some Mechanical Properties of Squeezed Aluminum 4% Copper

Author name: حنين محمد هادي
Supervisor name: حيدر عبد الحسن العذاري
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Babylon
First pages:

استقصاء قلف شجرة الكالبتوس كمانع تاكل للفولاذ الكربوني X52 في الاوساط المختلفة للانابيب الناقلة للنفط الخام == Investigation The Bark Of Eucalyptus Tree As Corrosion Inhibitor For Carbon Steel X52 In Different Media Of Crude Oil Pipelines

Author name: زينب فؤاد حمزة الشريفي
Supervisor name: كاظم فنطيل السلطاني
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Babylon
First pages:
Abstract: In the oil and gas industry, the crude oil pipelines which made of low carbon steel suffer from internal corrosion. The corrosion operation is originally related with the presence of the wastewater mixed with the crude oil, especially when it is accompanied by hydrogen sulfide, carbon dioxide, elemental sulfur, inorganic salts, organic acids, and bacteria. Corrosion inhibitors injection in the oilfield is a most common and beneficial method for prevention the pipelines internal corrosion. Because of a high cost and toxic nature of the chemical corrosion inhibitors which used presently in oil industry, it is necessary to promote a less expensive and environmentally acceptable inhibitors, natural plants can be treated as a perfect sources for this purpose.This study investigate the internal corrosion of low carbon steel pipelines in fluid environments, as well as prepare and use natural and locally available plant ( the bark of eucalyptus tree) as a natural corrosion inhibitor, and compared the new inhibitor with a chemical inhibitor used by Missan Oil Company (MOC) in terms of the cost, toxicity, availability and performance.Some experiments were achieved to estimate the performance of a new inhibitor, one of these tests include corrosion measurement by simple immersion in crude oil within and without of inhibitors which added in different amounts 30, 40, 50, and 60 ppm , where the best inhibition efficiencies which get when added the inhibitors in a critical amounts or closest to it, since for the aqueous extract (EB - A) the inhibition efficiency reached (94.4) and (86.71)% at 300 and 323K respectively, and for diethyl ether extract (EB - D) reached (82.87) and (84.6)% at 300 and 323K respectively, while the chemical inhibitor (CRW) which used by MOC reach to (84.21) and (88.73)% at 300 and 323K respectively.optical microscopy examination have been conducted to evaluate the corrosion nature where it show a clear difference in the topography of the immersed samples surface after add the inhibitors at two temperatures.Another tests was achieved to evaluate the corrosion behavior such as potentiostatic polarization and open circuit potential tests in wastewater, since the inhibitor efficiency at 313k reached (88.21)% when add a 60ppm from the EB - A inhibitor to the wastewater in Tafel extrapolation, while it reached (74.91)% when add a 30ppm from the EB - D inhibitor.Several tests was achieved such as FT - IR spectra and using a chemical reagents to detection the presence of many active groups and the presence of tannins, phenols and alkaloids in the Eucalyptus Bark (EB).The results show , that the new corrosion inhibitor is not only equivalent to a chemical inhibitor, but have greatly improvement properties such as : high efficiency , low cost , non - toxic , easily to product, and nonpolluting as compared with chemical inhibitor which is considered toxic and cancering inhibitor.

استقصاء الخواص الفيزيائية والميكانيكية لنحاس الومينا متدرج وظيفيا == Investigation Of Physical And Mechanical Properties Of Cu/Al2O3 Functionally Graded Materials

Author name: رؤى حاتم كاظم
Supervisor name: عبد الرحمن كاظم عبد علي
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Babylon
First pages:
Abstract: One of the most important smart material is the functionally graded materials, which had more increasing attention in different engineering applications.In this study, five - layered stepwise Cu/Al2O3 as functionally graded materials have been prepared from copper powder with five percentage of alumina powder as (5, 10, 20, 30, and 40 Wt%) by using powder metallurgy technique. Mixing of copper (34.32 ?m) and alumina (1.439 ?m) powders for two hours and then several disk sample with dimensions (14mm diameter and 10mm thickness) and cylindrical specimens with (18mm diameter and 27 height) have been compacting at different compacting stresses (550, 650 and 750 MPa). However, sintering of specimens for three hours at 850?C under vacuum about has been achieved.Several physical tests such as porosity, electrical resistance and thermal conductivity, X - ray diffraction, X - ray Fluorescence and Particale size analysis have been achieved. Furthermore, Microstructure and mechanical tests such as hardness, compression, double shear and dry sliding wear have been done for preparing samples from composite and functionally graded material.Numerical modeling using finite element analysis by ANSYS software has been presented for copper/alumina joints and compare with copper/alumina functionally graded materials.From the several experimental results, it is clear that the best compacting pressure was 650 MPa is determined by measuring green density at different compacting pressure, hardness increased with the increasing additive percentage of alumina, hardness resultschange in each layer by producing functionally graded materials (FGM) according to the percentage of the harder constituent (i.e. Al2O3) from 53 to 113 HV at compacting pressure 650 MPa, While the shear strength decreases with alumina increased from 72 MPa for layer one to 28 MPa for layer five at compacting pressure 650 MPa. The Wear rate increases as the time and load is increased. The wear resistance increased with increasing contain of Alumina. Results from the numerical modeling, it is clear that residual thermal stresses gradually decreased from the interface to the edges of functionally graded sample whereas in Copper/Alumina joint there is very high thermal residual stress in the joint interface.

امثلية عمليات اللحام باستخدام مصفوفة التضارب == Optimization Of Welding Processes Using Confusion Matrix

Author name: حسين خليل برهان
Supervisor name: حيدر الجبوري
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: English
University location: Babylon
First pages:
Abstract: Welding is a materials joining process in which two or more parts coalesced at their contacting surfaces by suitable application of heat and/or pressure.The proposed system consist of three stages : - First stage : preparing the actual samples from the previous research. These stage have multi tests (i.e, residual stress, fatigue life, impact energy, hardness and tensile strength) - Second stage : Translated the result of previous stage depending on speed of welding and heat input. The mechanical properties was related to the heat input and the temperature of the processes of welding. The quantity of the heat input was increased when the speed of welding was slow and heat input decrease when the speed of welding was high, this high heat input led to form coarse grain and this led to decrease the mechanical properties.Third stage : generated software system used different types of error measures, this software include two phase, the first phase is to estimate the error between the actual and predicted tests. While the second phase is to verification of the result phase on the person correlation measures, and this phase show high correlation among welding processes. In general these correlation lied from +1. The verification occur base on the measures of confusion matrix, (i.e SSE, MSE, RMSE ,MAPE, MPE and MAE ).The system satisfy the following results (Accuracy equal 84.37%, True positive (TP) equal 86.66 % and Precision equal 96.2% ).

تاثير معدل التبريد على خواص سبيكة Ag - Cu - Sn == Effects Of Cooling Rate On Roperties Of (Ag - Cu Sn) Ternary Alloy

Author name: جمان حيدر ساجت
Supervisor name: حيدر حسن جابر جمال الدين
Specific topic: Metals Engineering
Degree: Higher Diploma
Language: English
University location: Babylon
First pages:
Abstract: Dental fillings is widely used because of good mechanical properties and low cost but also was one of the more fillings topic of discussion and it studied continuously.The objective of this research is studing the effect of the cooling rate on the phases and properties of amalgam. two alloys were prepared by two types of casting (die casting and sand casting) with fixed percentage of tin, copper, silver and zinc for both alloys respectively about (7.5gm, 6.25gm , 10.75gm , 0.5gm).The process done by using an electric furnace in an inert gas atmosphere of argon and alloys thermally treated at a temperature (400C?) for a period of four hours for the purpose of homogenization phases alloys. And then it was studying the microstructure using an optical microscope. And using X - ray diffraction to determine the phases in alloys.The phase evaluation showed that the phases in the amalgam alloy (die alloy) has ? (Ag3Sn) , ? (Cu3Sn), and one other phase ? (Cu6Sn5) and the phases in the amalgam alloy (sand alloy) has ? (Ag3Sn) and ? (Cu3Sn). Then alloys have been converted into powder using a ball mill. The powder was treated thermally output for temperature (100C?) for a period of three hours atmosphere vacuum to remove internal stresses.The amalgam manufactured according to the ADA specification No.1 where he was mixing 0.8gm from each of the mercury and the powder for 30 seconds mined device and then put the dough, resulting in the mold of Teflon and sheds them straining compression amount (14MN / m2) for a period of 85 seconds still stress after that, the sample isextracted from the mold after the half - hour and placed in a glass chamber at a temperature of 37 ± 1C?.Microstructure of the amalgams were studied primarily by x - ray diffraction, optical microscopy.The phase analysis of two amalgams shows two phases; ?1, ?.studied the mechanical properties (tensile, compression, creep, dimensional change, hardness) and the result was that all properties effected with the change of the colling rate.It was conducted two types of corrosion tests are testing the open circuit (OCP) and potentiodynamic polarization in industrial saliva solution at a temperature of 37 ± 1C?.

تاثير اضافة الكالسيوم على البنية المجهرية والخواص الميكانيكية لسبيكة Al - Cu - Mg == Effect of Ca Addition On The Microstructure And Mechanical Properties of Al - Cu - Mg Alloys

Author name: نور صباح توفيق
Supervisor name: منذر محمد راضي
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: في هذه الرسالة تم دراسة تاثير اضافة عنصر الكالسيوم بنسب مختلفة ) 3.0 المجهرية والخواص الميكانيكية لسبيكة) المنيوم - نحاس - مغنيسيوم ( , حيث تم انتاج هذه السبائك باستخدام والتي تتضمن )المعاملة المحلولية, )? السباكة الرملية وعوملت حراريا باستخدام المعاملة ا | In this thesis ,the effect of pure Ca element addition in different percents of (0.3,0.6,0.9%) on the mechanical properties of Al - Cu - Mg alloy were studied.The Alloys were produced using sand casting and heat treated using T6 which involve [solution treatment , quenching , artificial aging ], aging process were carried out at 220? C for different periods of time ranging between (5min to5hr).Also the work involves a study on the effect of Ca addition on both grain size as well as the resulting phases before and after heat treatment, samples were examined using optical microscope, Scanning Electron microscope ,X - Ray diffractometer and image - J to estimate the average grain size.The results of hardness and tensile tests for 0.6% Ca and 4hr aging shows the best response as compared to the other alloys. The hardness and strength values have been changed from (78.29HV)(110.57Mpa) during (30min)at 220?C for non - Ca content alloy to(125.9HV)(164.2Mpa) for 0.6%Ca alloy. X - Ray diffraction , results shows the basic phase that forms is Al2CuMg (S??, S? phase) which is considered as the main strengthening phase in AL alloys, and it was found that Ca addition leads to form (Al4Ca) and (Al2Ca)which delay the alloy response to precipitation hardening by delaying the formation of (S)phase. SEM images showed a large and small dimple structure and broken or cracked Al - Ca compounds particles.This indicates that the fracture was ductile fracture in the Al matrix and brittle in these compounds ,.Also presence of microvoids (porosity) on the fracture surface is formed at the interfaces between Ca compounds and Al matrix enhanced the crack propagation through their center. The presence of the secondary phases precipitates (Al2CuMg ,Al2Ca and Al4Ca) in the fracture surface also contributed to ameliorate the mechanical properties by increasing the bonding of the matrix and reduced the ductility.Also Ca addition in the range of (0.3 - 0.6%) gives rise to grains refining ,While increasing Ca content up 0.9%wt coarsing the grains, which leads to decrease the hardness and tensile strength, From these results the decrease in tensile strength with increasing Ca content over 0.9% seems to be attributed to the reduction in elongation caused by the occurrence of micro porosity due to Ca addition.

دراسة سلوك البلى الترددي لمواد مركبة ذات اساس من سبيكة المنيوم / sic تحت ظروف الانزلاق الجاف والرطب == A Study On The Reciprocating Wear Behavior of Aluminum Alloy / SiC Composites Under Dry And Wet Conditions

Author name: عتبة حسين علوان
Supervisor name: احمد علي اكبر اكبر
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: تم في هذا البحث دراسة معدل البلى لاحدى سبائك الالمنيوم ((AA2024) (Al - Cu - Mg ومواد مركبة عن طريق تصنيع جهاز بلى ترددي تبعا للمقياس العالمي ( ASTM G133) ذو ترتيبة المسمار على المستوى (Pin on Flat) لمتغيرات مختلفة (الحمل المسلط , النسبة الوزنيه لدقائق كا | In this work the wear rate of one of aluminum alloys (Al - Cu - Mg) (AA 2024) and composite materials, has been studied by manufacturing a reciprocating wear device according to the International Standard (ASTM G 133 Pin on Flat) for different variables (applied load, weight percentage of (SiC) and sliding speed) under dry and wet (lubrication) conditions. Stir casting method has been used to prepare a composite material by using vortex technique to force the particles inside the molten metal (Al - alloy) and to distribute them regularly. The composite materials reinforced with different weight percentages of SiC (3, 6, 9, 12 wt%) are used. The base alloy and composite materials samples were tested to investigate the microstructure, and phases using optical microscope and Vickers hardness, wear rate, and the worn surfaces by using scanning electron microscope (SEM). From the results of microscopic examination it is found that the microstructure of alloy matrix was fine dendrites, in addition to the SiC particles that distributed near homogenously in the alloy matrix. The hardness test results showed that, the increasing of the weight percentage of (SiC) leads to increase the hardness, and the highest value of hardness was found at 12wt% SiC. Also the results showed that the wear rate increases with applied load for all weight percentage of reinforced particles (SiC).With increasing the load, more wear tracks, deep, and closed paths are formed and severe wear happens under dry condition but the lubrication case has less effect than dry case.It was shown that wear rate of both base alloy and composites under various conditions, increases with increasing of applied load and sliding speed but the wear rate decreases with increasing the SiC wt% in composite.Statistical method using software (Minitab 16) was used to study the effect of wear rate for both the base alloy and composite material by using three variables; applied load (X1), silicon carbide proportion (X2), sliding speed (X3), with five levels of each variable. It is concluded that the optimum weight loss under dry case was 0.0014g, The combined effect of variables and the wear rate was obtained and which variable are more influential, as shown in the equation below : D = 0.056703 - 0.002164 X2 - 0.000282 X3+ 0.000017 X1 X3 +0.000010X2 X3 While under lubrication case that the optimum weight loss was 0.0037g and the combined effect of variables and the wear rate was obtained and which variable are more influential, as shown in the equation below : L= 0.009607 + 0.002825 X1 - 0.002375 X2 + 0.001100 X3 + 0.001664 X3 2 + 0.004700 X1 X3 + 0.002700 X2 X3 The applied load (X1) and sliding speed (X3) have the largest effect on wear rate.

دراسة تجريبية حول مسحوق حبيبات النحاس ذات الحجم النانوي باستخدام الترسيب الكهربائي المصحوب بالامواج الفوق صوتية == Experimental Study of Nanosized Copper Powder Using Sonoelectrodeposition Process

Author name: حيدر ياسر ثامر الياسري
Supervisor name: محمد جاسم كاظم | عدنان شمخي جبر
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: عملية الترسيب او التحليل الكھربائي تعتبر من الطرق التصنيعية الرئيسية التي تستخدم لانتاج مختلف الاشكال والاحجام (ضمن المدى الميكروي) من حبيبات مسحوق معدن النحاس والتي تستخدم لاحقا بواسطة تكنولوجيا المساحيق لانتاج اجزاء محددة. ايضا استخدمت ھذه الطريقة بمد | Electrolytic or electrodeposition process is considered a main way to produce many shapes and sizes (micro range) of copper powder to be used in powder metallurgy process. It is used broadly to deposit copper coatings with nanosized grains, but it is rarely used to produce nanosized particles of copper. Reaching this goal is highly dependent on the optimum design of the parameters of electrodeposition process.This work aims to study the important variables that most affect the electrodeposition process outputs. These variables are : copper sulphate pentahydrate salt concentration CuSO4.5H2O (1, 5.5, and 10) g/l, cathodic current density (12.5, 25 , and 37.5) mA/cm2, ultrasonic (20 KHz frequency) vibration amplitude (5%, 20%, and 35%) from the maximum amplitude (1 ?m), and amount of sulphuric acid H2SO4 (H2SO4 concentration > 97%) in electrodeposition cell (0.05, 0.10, and 0.15) ml/l. The study of effects of these variables is concerned with size of resultant powder particles, also their effect on the purity, morphology, and shapes of particles is studied, and the crystallinity of particles is also covered.The design of experiment (DOE) approach is applied here through Taguchi design of experiments, to manage and analyze the results and study the specific effects of each. The arrangement of variables’ levels is done using the setup of (Taguchi L9).The analysis of experiment tests of the study of electrodeposition process to get copper nanoparticles showed that all variables have effect on the size of resultant copper particles, but in different ways and degrees. The mean particle size of all samples is about 86 nm. It was found that the increasing of concentration of copper sulphate salt (1, 5.5, and 10) g/l had a negative on the increasing the size of copper particles in the range (71, 69, and 117) nm.While the increasing of cathodic current density (12.5, 25 , and 37.5) mA/cm2 had an effect of decreasing the particle size of copper in the range (114, 75, and 68) nm. The case was the same for increasing of amplitude of ultrasonic vibration, where increasing it (5%, 20%, and 35%) caused decreasing in the particle size in the range (97, 92, and 68) nm. And the effect of acid amount (0.05, 0.10, and 0.15) ml/l was multiple because it decreased the particle size first and increased it later in the range (90, 65, and 102) nm. The amount of effect of each variable on the process was calculated using specific equations of Taguchi design. It was found that the current density has the bigger effect (35%) on the resultant particle size (it minimized the size). The salt copper concentration has the second effect (34%) (it maximized the size), and thirdly the acid concentration effect is 19% (it had multiple effect on the size).Finally the ultrasonic vibration has 12% effect (it minimized the size). The optimum values of process parameters that lead to minimum size of the particles were : CuSO4.5H2O concentration = 5.5 g/l, Current density = 37.5 mA/cm2, Ultrasonic amplitude = 35%, H2SO4 concentration = 0.1 ml/l.The SEM photographs were used to examine the morphology of particles. The results show that the shape and morphology widely vary between many modes : from treelike through irregular, angular, or rounded shapes to a wellfaceted truncated octahedron. The forming of well - faceted truncated octahedron copper particles is related strongly to the presence of ultrasonic vibration which plays the role of inhibitor.Energy dispersive spectroscopy (EDS) elemental analysis of copper nanoparticles indicates the high purity of most of samples except the cases where there are traces of oxygen from very thin layer of oxides and/or carbon from residual alcohol.The x - ray diffraction studies reveal that the resulting particles are a crystalline copper element with a face center cubic (FCC) crystal structure.

تاثير المعاملة بالليزر على مقاومة التاكل للفولاذ المقاوم للصدا نوع 304 == Effect of Laser Treatment On Corrosion Resistance of 304 Stainless Steel

Author name: زمن عبد الرزاق عبد الوهاب
Supervisor name: محمد جاسم كاظم | سامي ابراهيم جعفر
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: تعتبر هذه الدراسة بانها محاولة لتحسين مقاومة التاكل للصلب المقاوم للصدا من نوع 304 عن طريق الانصهار السطحى بالليزر. تم استخدام تقنية منحني تافل لتحديد معدلات تاكل الصلب المقاوم للصدا نوع 304 في محلول 3.5? كلوريد الصوديوم عند اربعة حالات مختلفة. الاولى بدو | The present work represents an attempt to improve corrosion resistance of sensitized 304 stainless steel by laser surface melting treatment. Tafel extrapolation technique was used to determine the corrosion rates of stainless steel type 304 in 3.5% NaCl in four conditions. The first condition is as received, the second sensitized microstructures at temperatures 850 oC for one hour, the third condition is treating the stainless steel alloy by laser surface melting (LSM) without sensitization. The fourth condition is studying the effect of LSM on sensitized stainless steel.The main results obtained are expressed in terms of corrosion parameters through electrochemical behavior : E°, I°, E Corr., ICorr., EP., IP, EPit. and IPit.These parameters are strongly dependent on the microstructures of the alloy. The results reveal when the potentials increase, this means that the microstructure becomes thermodynamically more stable and has good corrosion resistance. The above electrochemical parameters for sensitized 304 stainless steel show that localized corrosion rate increases due to precipitation of chromium carbides on grain boundaries and to the sensitization process affecting the phases. The LSM treatment shifts the potential toward noble direction, the corrosion current densities values shift to lower values. Generally, a change in surface hardness shows a microstructure modification in metallic bonds. The comparison of anodic polarization curves indicates that the corrosion rates for laser treated specimens are reduced. Increase in corrosion resistance probably means that most inclusions at the surface have been dissolved in the structure due to melting or alternatively, they are covered by molten materials. An interesting feature is the systematic shift of the pitting potential in the noble region with a laser treatment. This result confirms that the laser treatment can be used successfully to improve the localized corrosion resistance.

دراسة الخواص الترايبولوجية لمادة متراكبة ذات اساس نحاس == A Study of Tribological Properties of Copper Matrix Composite Material

Author name: مريم عبد العظيم باقر
Supervisor name: اسراء عبد القادر عزيز
Specific topic: Metals Engineering
Degree: Master
Language: Arabic
University location: Baghdad
First pages:
Abstract: يهدف البحث الى دراسة مقاومة البلى والاحتكاك للمادة المتراكبة ذات اساس نحاس من نوع ? - براص (Cu - 29.5%Zn) والمقواة بدقائق من كاربيد السليكون مرة ودقائق من الكرافيت مرة اخرى. وكانت نسب الاضافة wt%(5، 10، 15) لكل منهما. لقد تم تصنيع هذه المواد المتراكب | This research is devoted to study the wear resistance and coefficient of friction of copper matrix composite type - brass (Cu - 29.5%Zn) which reinforced with silicon carbide particles in one state and graphite particles in another and the addition percent was (5,10,15) % for each. Preparation of composite materials carried out by stir casting using vortex technique.A study of adhesive wear resistance was carried out by using the pin - on - disk technique for the base alloy and composites materials in different conditions by measuring the coefficient of friction and wear rate as well as the effect of each factor from applied load and sliding speed and type of composites.Three loads (5,10,15) N were used at constant sliding speed 3.7 m/sec. as well as three speeds (2.7 , 3.7 , 4.7) m/sec were used with constant applied load at 10 N.The results showed that the wear rate is increase in general with increasing the applied load , but the composite material reinforced with graphite particles showed wear rate lower than that of the base alloy and the composite material reinforced with silicon carbide particles. While, when different sliding speeds were used , the results showed that the wear rate is decrease with increasing sliding speed. It is clear that the composite material reinforced with graphite particle has small wear rate and coefficient of friction as compared with base alloy and composite material reinforced with silicon carbide. It is clear from coefficient of friction that it is increase with increasing the time until the It is clear from measuring the change in surface temperature for each one of materials the base alloy and composites materials under the effect of different loads (5, 10 , 15) N and at constant sliding speed 3.7 m/sec , rising in temperature is noted with increase the value of applied load and the composite material reinforced with graphite particles showed remarkable decreasing in temperature as compared with base alloy and composite material reinforced with silicon carbide.

دراسة تاثير سرعة الدوران ودرجة الصب على توزيع السليكون في سبيكة Al - 23% Si بسباكة الطرد المركزي == Study The Effect of Rotation Speed And Pouring Temperature On The Distribution of Si In The (Al - 23% Si) Alloy Produced By Centrifugal Casting

Author name: عبد الجبار سعد جمعة
Supervisor name: نوال عزت عبد اللطيف | رابحة صالح ياسين
Specific topic: Metals Engineering
Degree: Master
Language: Arabic
University location: Baghdad
First pages:
Abstract: يهدف البحث الى تحضير مادة متدرجة وظيفيا" ( FGM ) باستعمال طريقة السباكة بالطرد المركزي ودراسة تاثير متغيرات العملية على البنية المجهرية لسبيكة المنيوم - سيليكون فوق اليوتكتك (Al - 23%Si ). تمت دراسة تاثير كل من سرعة دوران قالب السباكة ودرجة حرارة الصب ( ا | The aim of this study was to prepare a functionally graded material by using centrifugal casting method and study effect of parameters process on the microstructure of a hypereutectic ( Al - 23%Si) alloy. Effect the rotation speed of mold casting and overheating temperature on the microstructure and hardness of ahypereutectic ( Al - 23%Si) alloy were investigated. Therefore, the melt was overheated to( 800,900) C? and poured in the centrifugal casting mold after preheating by used gaseous torch to (100) C?. Then we obtained on cylinders at different rotation speed (765,840,1043,1712,1878) r.p.m. Optical microscopy and scanning electron microscopy used to study the microstructure to produce samples. The results showed that the overheating temperature and mold rotation speed affect on the grain size and volume fraction of ( ? - Si) phase, increasing of the overheating temperature due to increasing average volume fraction and decreased the grain size of primary silicon, but increasing mold rotation speed due to increasing the average volume fraction in the inner layer from cylinder thickness and decreased in the intermediate and outer layer , also decreased the grain size of primary silicon. The maximize volume fraction was in the inner layer from a cylinder thickness obtained at rotation speed (1878) r.p.m. and poring temperature (900)C? , where the values of volume fraction of ( ? - Si) phase are (35%) and obtained on completely functionally graded material. The results of micro structural observations showed that centrifugal casting process contributed to change the eutectic phase morphology from coarse needle - like structure to fibrous structure at increasing mold rotation speed but increased pouring temperature due to invert, and the results showed found thickness of (Si) particles in the metallic matrix decreased with increased rotation speed. The results of hardness tests to a cylinders samples showed maximum hardness values in the inner layer from cylinder thickness and increased with increasing mold rotation speed but it is decrease with increasing rotation speed. values hardness in all layers decrease with increasing pouring temperature. The results of wear tests showed maximum wear resistant was in the inner layer from cylinder thickness at rotation speed (1878) r.p.m. and poring temperature (800)C? and then coming outer layer but minimum wear resistant was in the intermediate layer.

المعاملة السطحية بالليزر لحديد الزهر الرمادي باستخدام ليزر (Nd : YAG - Nano Second) == Laser Surface Heat Treatment For Gray Cast Iron Using Nano Second Nd : YAG Laser

Author name: بلال احمد حبيب
Supervisor name: رابحة صالح ياسين | هجران زين العابدين طعمة
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: في هذا البحث، تم استخدام تاثير معلمات الليزر لتحسين الخواص السطحية للحديد الزهر الرمادي، وذلك باستخدام جهاز Nd : YAG ليزر بطول موجي nm(1064 (، البعد البؤري cm( 5 ,10,18)، وامد النبظة ns (10). استخدمت طريقة الانصهار السطحي بالليزر في تصليد العينات، الى | In this thesis , the effect of laser parameters is used for perfection of the surface characteristics for gray cast iron , using pulsed Nd : YAG laser with wavelength of (1064nm ).The laser surface glazing and shocking methods have been used in hardening the specimens , besides using the laser energy in treatment of (1.2 J) , pulse duration (10 ns), with different focal length of (5,10,18) cm and used the (air ,water , DMSO) as a active medium. In laser surface engineering the micro hardness, roughness and wear rate examinations deliberated before and after laser treatment. The effect of laser parameters includes : The effect of the pulse repetition rate (P.R.R) , the result shows , thevalue of the micro hardness of work pieces reduced but the variation in the value hardness decreased. For the effect of the medium used (air, water, DMSO) it was found with increasing the water and DMSO high the value of the micro hardness of work piece increased and value of the (loss of weight , wear rate, surface roughness ) reduced. After treatment by laser the amount of loss in weight is less than the loss of weight with the base metal (before the treatment) , so the results reveal an improvement in wear rate after treatment by laser. And for the effect of overlapping technique ,it was found that the best percentage for overlapping technique ratio is 50% for the selected laser energy. The value of micro hardness increased by moving away from the center of the laser strike on the work piece.

تاثير اضافة عنصر النيكل الى سبيكة Al - 4% Cu - 1.5% Mg == The Effect of Ni Addition To Al - 4 % Cu - 1.5% Mg Alloy

Author name: اسيل احمد اموري
Supervisor name: منذر محمد راضي
Specific topic: Metals Engineering
Degree: Master
Language: Arabic
University location: Baghdad
First pages:
Abstract: في هذا البحث تم دراسة تاثير اضافة عنصر النيكل النقي وبنسب مختلفة (wt % 5 - 3 - 2 - 1) الى منصهر سبيكة المنيوم - نحاس - مغنيسيوم وتمت سباكتها بوساطة السباكة بالقوالب المعدنية ومن ثم اجراء المعاملة الحرارية التي شملت (عملية التجانس الحراري على السبائك بعدها | The studying effect of adding pure nickel element in different percentages to (Aluminum - 4%Copper - 1.5%Magnesium) during alloy molten state by die casting procedure, and then make the heat treatment that includes : (the thermal homogenizing followed by heat treatment (T6) which includes solution treatment followed by artificial aging at 220 C? at different times within the range (30 min. - 5 hr.)). Also had been studied the effect of pure nickel element on microstructure and on grain size and the types of phase that created in alloys produced by founding by using optical microscope , x - ray diffraction test device and a program that calculates the volume fraction of particles (J - image). So when we tested the hardness, the result showed that the alloy with highest adding rate (5% wt) have the best response between other alloys for hardening in longer time period and we reached to highest hardness (125 H.V) in time period (4hr) at (220 C?). While the alloy that doesn't have nickel reached to highest hardness equal to (112 H.V) in time period less than (2hr). The phases that created in alloys had been listed through analysis the x - ray diffraction and study the microstructure; we found the phase (Al7Cu4Ni) that be responsible on showing in alloy's response to precipitation hardening which leads to delay, also we found that the adding of nickel causes increase and improve in properties of tensile strength, yield strength and elongation, this is belong to presence of nickel that takes two ways, a part of it dissolves with Aluminum and copper and produce the phase (Al7Cu4Ni) which slows producing the phase (Al2CuMg), and other part refining grains size at highest temperature degrees that leads to increase in strength and hardness with higher rates for alloys contain nickel in comparison to those empty of nickel.

الحماية من التاكل لقواعد الاعمدة الكهربائية في الترب ذات المقاومية المنخفضة == Corrosion Protection of Electrical Bar Stands In Low Resistivity Soil

Author name: اياد نصيف جاسم
Supervisor name: سامي ابراهيم جعفر الربيعي
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: يستخدم الفولاذ المغلون في تصنيع الاعمدة الكهربائية لامتلاكه خواص ميكانيكية جيدة ومقاومة تاكل عالية. وتحت الظروف الاعتيادية يعاني العمود من التاكل بعد عدة سنوات من الخدمة.يصنع عمود الكهرباء من فولاذ St - 52 والمطابق للمواصفة DIN الالمانية ويتالف من ثلاثة | Galvanized steel is used in electrical poles because of the good combination of its mechanical properties and the corrosion resistance. Under normal conditions, electrical pole suffered from corrosion after some years in service. Electrical poles, which were made according to Germany standard DIN st.52, consist of three parts; the upper, mid and lower part. This study focuses on the last part because the surrounding soil of electrical pole is more corrosive than the atmospheric environment, which surrounds to other two parts of the electrical pole. Soil resistivity is the one variable that has the greatest influence on corrosion rate. Electrical poles which at buried in low resistivity soils will generally be anode, whereas electrical poles buried in adjacent high resistivity soils will generally low corrosion.The electrolyte in this work was prepared according to the values of Iraqi soil resistivity. Sodium chloride (NaCl) was used in different concentrations of (2, 2.5, 3 and 3.5) wt. %, which are equivalent to 27, 24, 20 and 18 ohm.cm. Two methods were used in this work in order to improve corrosion resistance, the first method galvanizing process in different thicknesses (80, 90,100,110,120 and130) µm and the second method is coating by different types of Iraqi paints (D - 5547) with hardener (H - 1457)and(G - 5532,G - 5533,D - 5542) with hardener(H - 5533) The corrosion rate and corrosion potential of steel increases and decreases with the increase in NaCl wt.% concentration respectively. Corrosion rates (mpy) with coating thickness are achieved as a function of environment in different soil resistivities. The more corrosion resistance occurs at 120 µm galvanized layer. Micro cracks appear at 130 µm galvanized thickness.In this work, two mixed ratios of paint and hardener were used. These ratios are 2 : 1 and 1 : 1. Paint with mixing ratio equal to 2 : 1 of G - 5532 + G 5533and mixing ratio 1 : 1 D 5542 with hardener 5530 gave the more corrosion resistance.The coating thickness has a direct influence on the performance or life of the electrical pole. As the thickness of galvanized layer increases, the life of protection increases until 120 µm. The life of a zinc coating is a linear function of coating weight for any specific environment. The efficiency of coated electrical pole either by galvanization or paint process was a proximately between 94% to 97% and 98% to 99.6% respectively.

متغيرات اللحام المثلى بالقوس الكهربائي المغمور باستخدام طريقة تاكوشي == Optimizing of Submerged Arc Welding Parameters Using Taguchi Method

Author name: هشام جواد كاظم
Supervisor name: احمد علي اكبر اكبر
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: اللحام بالقوس الكهربائي المغمور غالبا مايستخدم في الصناعات الثقيلة. يستخدم في هذا النوع من اللحام سلك لحام مستمر يكون معدنن الملئ. االقوس يكون مغمور في مساعد الصهر والذي يتم تغذيته من خلال انبوب في حاوية اعلى سلك اللحام الذي يغذى باستمرار. مساعد الصهر يع | Submerged arc welding (SAW) is often used for heavy industries. The SAW process employs a continuous bare wire electrode that is consumed to produce filler, the arc is submerged in the flux, and the flux is supplied through a funnel located ahead of the filler wire which is fed continuously from a hopper, the flux contributes to deoxidize the base metal, and protect the molten weld metal from atmospheric contaminants In order to achieve best weld quality and good mechanical properties in manufacturing industries which need to be optimized. Selection of appropriate SAW parameters is essential to ensure a predictable weld bead which is important for obtaining high quality welding.Manufacturing industries and training centers often face the problem of selecting appropriate or optimum combinations of input welding parameters for achieving the required weld quality. Three input parameters of SAW were used to weld the steel plates, and four levels for each parameter, and three output response variables were used The experimental work consists of welding of sixteen low carbon steel plates of (AISI 1005) specimen measured 300 mm × 50 mm × 12 mm were submerged arc welded using welding currents (280, 340, 400, 460) amp, voltage (26, 29, 32, 35) volt and welding speeds (3.3, 5, 6.6, 8.3) mm/s This work details the application of Taguchi design to determine the optimal SAW parameters. An effort has been made to study the effect of SAW process parameters (current I, voltage V, speed S) on the bead geometry dimensions (depth of penetration P, bead width W, heat affected zone width w).Signal to noise ratios are computed to determine the optimum parameters. Statistical models have been developed based on multiply regression analysis relating the bead geometry with process parameters. The adequacy and significance of the models were checked by using ANOVA technique, also the models are validated using normal probability plot, and residual versus fit plots.The models were employed easily in form of executed program designed by using Visual Basic 6 software. The objective of such models and designed program is to predict weld bead geometry which enables selecting the desired weld parameters and select the weld bead dimensions. The effect of SAW parameters on heat affected zone and weld metal hardness also has been studied by means of hardness measurements, and grain size measurement using intercept method. Main and interaction effects of the process parameters on bead geometry are presented graphically. The experimental results were analyzed by using Minitab 16 software.It was found that current (280 to 460) amp causes increase in depth of penetration from (1.742 to 3.752) mm and HAZ width (1.222 to 1.512) mm. Bead width increases from (10.99 to 13.13) mm with increase in voltage from (26 to 35) volt and decreases from (12.61 - 11.80) mm with increase in welding speed from (3.3 to 8.3) mm/s. The welding speed and voltage do not affect appreciably the depth of penetration. Also change in weld speed reduces the width of the HAZ from (1.462 to 1.295) mm. The hardness of HAZ reaches maximum value 122.39 HV at the center of HAZ and decreases gradually toward the BM 109.22 HV; also it was found that the executed program is a useful tool used to predict weld bead geometry dimensions from welding parameters for SAW process.

دراسة العوامل المؤثرة في خواص مسحوق القصدير المنتج بطريقة التذرية بالطرد المركزي == Study of The Factors Effecting The Properties of The Tin Powder Produced By The Method of Centrifugal Atomization

Author name: علي حسين علي كريم
Supervisor name: منذر محمد راضي
Specific topic: Metals Engineering
Degree: Master
Language: Arabic
University location: Baghdad
First pages:
Abstract: يتضمن البحث دراسة بعض متغيرات عملية التذرية بالطرد المركزي لغرض انتاج مسحوق معدن القصدير النقي وملاحظة مدى تاثير هذه المتغيرات في خواص المسحوق الناتج وهذه المتغيرات هي : - 1. سرعة دوران الجزء الدوار2. وسط التبريد3. درجة حرارة وسط التبريد تم ملاحظة تاثي | The research included a study for the variables of the process of centrifugal atomization for the purpose of producing pure tin metal powder and the effect of these variables in the properties of the resulting powder. These variables are : 1. The speed of rotation in the rotating part. 2. The medium of cooling. 3. The temperature of medium of cooling. The affect of these above variables were observed on the size and the shape of particles resulting and the particle distribution, the apparent density, tap density and the angle of repose. Upon the use of three different speeds (2000, 6000, 10000) (rpm) on the each at a time for the rotating of the hollow bowl and the use of water at the room temperature. It was noticed that when increasing of revolution speed, there is no change in the shapes of particles i.e. the wide extent of shapes remain irregular, acicular and semispherical, and that the weight percentage of the small particles increases. Also, the value of the apparent density and the tap density increases while the angle of repose decreases. It was also observed that at the use of air and water separately at the room temperature as cooling media and disintegration the fused droplets of tin metal out of the hollow bowl at rotation speed of (10000) rpm. Moreover, we can notice that the weight percentage of the small particles increases as well as the value of the apparent density and tap density, while the value of the repose angle decreases , and the absence of any change in the shape of the particles when using water as a medium of cooling , compare with air. A great range of irregular, acicular and semispherical shapes are also obtained. Water of different temperatures ({40 - 50}, {60 - 70}, {80 - 90})? C were was used as a cooling medium and for the disintegrating of the droplets of the tin metal from the hollow bowl at rotation speed of (10000) rpm, and the formation of powder of different sizes and shapes. Also, the tendency of the particles towards regularity of shape and the spherical shape clearly with the decrease of the weight percentage of the small particles , and the value of apparent density and the tap density increase and the value of the angle of repose decreases at the increase of the temperature of water cooling medium.

دراسة التاكل الميكانيكي الجاف لمادة متراكبة ذات اساس (SiC / Al - 4% Cu) == Studing Dry Mechanical Corrosion For Composite Material of Base (Al - 4% Cu / SiC)

Author name: وليد تركي راشد
Supervisor name: احمد علي اكبر اكبر | هجران زين العابدين
Specific topic: Metals Engineering
Degree: Master
Language: Arabic
University location: Baghdad
First pages:
Abstract: تم في هذا البحث دراسة مقاومة البلى لمواد متراكبة معدنية ذات اساس من الالمنيوم (Al - 4%Cu) باستخدام جهازذو ترتيبة المسمار على القرص (Pin on Disk) وتحت ظروف اختبار مختلفة هي (الحمل المسلط , نسبة اضافة دقائق كاربيد السليكون ,سرعة الانزلاق , زمن الانزلاق).حيث | In this research (study) wear resistance of composite materials based on metal, aluminum (Al - 4%Cu), has been studied under different test conditions (applied load, the proportion of added silicon carbide particles, a speed of sliding, sliding time) using a pin on the disk technique. Composite materials prepared using stir casting method, where vortex technique help to draw the ceramic particles into the molten metal and distributed uniformly. The composite materials containing 4 wt% Cu and 1 wt% Mg, reinforced with different proportions wt% SiC (3,6,9,12) were cast in a metal mold. Magnesium was added to improve the wetability between SiC particles and the aluminum matrix. The base alloy and composite materials samples were tested to investigate microstructure, phases, and properties using Optical Microscope, X - Ray Spectrometer, Vickers Hardness, and Scanning Electron Microscope. The optical microscope and scanning electron microscope (SEM) are also used to study the effect of loads on the worn surface. From the results of microscopic examination on found that the alloy structure of the foundation is a fine dendrite structure (Dendrite), and after the addition of ceramic particles leads to an improvement in microstructure, in addition to distributed almost homogeneous in the matrix and on the boundaries crystalline. X - ray diffraction examination approved the existence of aluminum and silicon carbide phases. In addition to the deposition phase (Al2Cu) because of the natural aging,(Mg Al2Cu) phase and the presence of this freak indicate on the interaction of aluminum with the added elements, The hardness test results show that, the increasing the ceramic particles proportion tend to increase the hardness, the highest hardness found at 12wt% SiC. By studying the worn surface, using optical microscope and SEM, increasing in wear was observed with applied load for all reinforced particles percentage added. With the increased load, more wear, deep, and closed paths was formed. Twotypes of wear were monitored at high loads, adhesive wear and abrasive wear. The studying of wear rate for both base alloy and composites materials with various conditions, show that wear rate increase with increasing applied load, but the composite materials show higher wear resistant. The best wear resistance found at 12 wt% SiC addition.The studying of sliding speed show that the wear rate decreases with high speed the for both base alloy and composites materials. The sliding time show direct correlation with wear rate, but at continuous increasing sliding time, wear rate decline constantly.Statistical methods with software (Minitab 15) was used to study the effect of wear on weight loss for both the base alloy and composite material by using three variables; ( applied load (X1), silicon carbide proportion (X2), sliding distance (X3), with five levels of each variable. It was concluded that the optimum weight loss (Optimization of weight loss) (0.0046 g), as a result the wear process, are found at the these following levels of variables; applied load (2.5 N), sliding distance (7.2 Km) and at the silicon carbide proportion (3.6364 wt% Sic). Equation describes the combined effect of variables and the weight loss was obtained and which variable are more influential. Y = 0.010180 + 0.002825 X1 - 0.002375 X2 + 0.001100 X3 + 0.001809 X32 + 0.004700 X1 X3 + 0.002700 X2 X3 The applied load (X1) and sliding speed (X3) both have the largest effect on weight loss. Both, applied load and silicon carbide does not have any effect on the weight loss. For individual variable, it foundthat applied load has the greatest influence on weight loss.

دراسة انتقال الحرارة لمسبوكات المواد المنتجة بطريقة الطرد المركزي == A Study of The Heat Transfer For Alloys The Materials Produced By Use Centrifugal Casting

Author name: محمد قاسم محسن
Supervisor name: نوال عزت عبد اللطيف | كريمة اسماعيل عموري
Specific topic: Metals Engineering
Degree: Master
Language: Arabic
University location: Baghdad
First pages:
Abstract: تم كتابة برنامج حاسوبي بلغة فورتران (90) لدراسة الانتقال الحراري لبعدين(2 - D) بطريقة الفروقات المحددة المباشرة (Explicit Finite Difference Method) للمسبوكات ( Al - 4.5%Mg)،(Al - 7%Si)،المنتجة بطريقة السباكة بالطرد المركزي الافقية، اذ تم حساب سرعة دوران | Mathematical program writing completion by Fortran 90 to study the heat transfer in two dimensions(2 - D) by use explicit finite difference method for two alloys(Al - 4.5%Mg),(Al - 7%Si),this alloys were produced by the horizontal centrifugal casting, The mold rotation speed for the centrifugal casting was calculated and it was put in the mathematical program at the change of the mold rotation speed N=(100,1000,1500)rpm. And study the effect of the change of the mold rotation speed on the cooling rate and microstructure and hardness. We input to the mathematical program the boundary condition of the mold from (temperature ambient and heat transfer coefficient by convection of the alloys external)and input thermal physical properties of the alloys from (coefficient thermal conductivity of liquid and solidus,density of liquid and solidus, solid fraction, , specific heat of liquid and solidus, liquid temperature, latent heat of solidification, solidus temperature, alloys melting temperature),then we melted the alloys by use electric furnace and poured the melting alloys in the centrifugal casting mold after proceeding heating prematurely to the mold by used gaseous torch and fixing(digital thermal couple). We input to the mathematical program. And study the difference in mold rotation speed and it’s effected on the cooling rate of the both alloys and the mold and microstructure and hardness , and study the difference in the mold material effected on the cooling rate of the both alloys, and study effected the mold heating on the cooling rate of the both alloys. As a result we noted that the solidification time of the alloys is dependent upon the speed of rotation of the mold.

دراسة سلوك البلى الانزلاقي الجاف لسبائك المنيوم - 7% سليكون عمليا وباستخدام تقنية تصميم التجارب == Studying Dry Sliding Wear Behavior of Al - 7% Si Alloys Using Experimental And DOE Techniques

Author name: قاسم سعد عبد الواحد
Supervisor name: عقيل ظاهر صبحي | علي عبار خليف
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: تعد سبائك الالمنيوم - سليكون والتي تحتوي على التيتانيوم احدى المواد التي تتميز بمقاومتها للبلى كما بينت الدراسات والابحاث العلمية ذلك.في هذا البحث تم صب سبيكة المنيوم - 7% سليكون وبنسب مختلفة من التيتانيوم (0.5 , 1 , 1.5%) وتحت معدلات تبريد مختلفة في قال | Aluminum - silicon alloys that contain Titanium can be considered one of the wear resistant materials and attract several researchers recently.In this work ,Al - 7%Si alloy with different percentages of Ti ( 0.5 , 1 , 1.5% ) was poured under different solidification conditions into the metal mould.All prepared alloys were dry slided under different bearing pressures ( 5 , 10 , 15 , 20 , 25 N ) on the steel counterface surface using pin on disk wear apparatus. Optical microscope and scanning electron microscope (SEM) were used to study the microstructure and determine wear mechanism of Al - Si alloys respectively. On the other hand , X - ray diffraction technique (XRD) was used to determine the phases that were present in the matrix of Al - Si alloys.Microstructural analysis and X - ray diffraction showed that two phases are presented in the matrix of Al - 7%Si alloys.These phases are ? - aluminum and eutectic and three phases are present in the matrix of Al - Si alloys that contains Ti. These phases are ? - aluminum ,eutectic and titanium aluminide Ti9Al23.Significant refinement occurred for ? - aluminum, eutectic and titanium aluminide Ti9Al23 phases when using metallic mould cooled with cold water in comparison with heated and unheated metallic moulds Hardness was increased with increasing Ti percentage and with increasing the severity of solidification condition used.Remarkable changes in the wear rate occurred for Al - Si alloys during dry sliding in which the magnitude of wear rate was dependent on the Ti percentage ,load and solidification condition used.Design of experiment (DOE) was used to optimize the effect of process variables ( load and Ti percentage) on the wear rate under different solidification conditions using computational statistical software (Mintab 16).

تاثير التشكيل على البنية المجهرية وسلوك البلى للمواد المعدنية المتراكبة النانوية Al2O3 / A356 == The Role of Forming On Microstructure And Wear Behavior of Metal Nano Composite Al2O3 / A356

Author name: مروان باسل حسين
Supervisor name: نوال عزت عبد اللطيف | عقيل ظاهر صبحي
Specific topic: Metals Engineering
Degree: Master
Language: English
University location: Baghdad
First pages:
Abstract: في هذا البحث تم تحضير المواد المركبة النانوية اساس معدني (A356/Al2O3) باستخدام تقنية (rheocasting) ومن ثم تم اجراء عملية التشويه على الساخن عند درجة حرارة °250 م.في البداية تم صهر السبيكة A356 في درجة حرارة °730 م بعدها تم تبريدها الى درجة حرارة الشبه ص | In the present work Al2O3/A356 nano composites have been prepared using rheocasting technique, the nano composites were then processed using hot deformation at 250 °C.Firstly A356 matrix alloy was melted at about 730 °C, the superheated molten alloy was allowed to cool to the semi - solid temperature at 600 °C, then Al2O3 nano - particles with different size (10,20) nm and different weight percentages (1 and 2)%wt were added inside the vortex formed due to stirring , hot deformation carried out with different ratio 30% and 40% at the temperatures of 250 °C and strain rates 0.1 s?1. The produced nano composites samples were characterized using optical and scanning electron microscopy ,X - ray diffraction , hardness test and wear test using pin on disc apparatus. The results of microstructural observations showed that the Al2O3 nano particles cluster mostly near the grain boundaries and form a band surrounding the grain boundaries. The dendritic structure of ? - Al phase is fragmented and the ? grains became more uniform and smaller than their corresponding as - cast 356 alloy. On other hand the microstructures of nano - Al2O3/A356 composites after casting and hot deformation at 250°C, showed modification of ? - Al and Si eutectic. The columnar dendrites ? - Al phase changed to the nearly equiaxed grains or globular morphology. The results of hardness test showed that the nano Al2O3/A356 composite were exhibited higher hardness than the as - cast A356 alloy The nano - composites hardness, increase with increases the size and increases in weight percentage of the Al2O3 nano - particles, and with increasing percentage deformation. The result of wear test showed that the hot deformed nano Al2O3 /A356 composites have greater wear resistance compared with hot deformed A356 alloy. Furthermore, with increasing the particle size and the percentage of Al2O3 nano particles, wear rate will decrease. The results also revealed that the optimal results was achieved at the nano - composites containing 20nm Al2O3 particles after hot deformation with 40%. SEM studies of the worn surface of nano composites showed that the main wear mechanism was oxidative in conjunction with metallic wear.
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