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Reduction of H2S Emission to The Atmosphere from Refinery Tail Gases

Author name: Firas Ismaeel Mousa
Supervisor name: Neran K. Ibrahim
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Higher Diploma
University: University of Technology - Department Of Chemical Engineering
Language: English
University location: Baghdad
First pages:

دراسة هيدروداينمكية على برج تميع عكسي ثلاثي الطور == Hydrodynamic Study on Three-Phase Inverse Fluidized Bed Column

Author name: نسمة بلاسم احمد
Supervisor name: زيدون محسن شكور | عامر عزيز عبد الرحمن
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:

دراسة سلوك نظام عملية التمييع باستخدام الدقائق النانوية == Study of Fluidizing System Behavior Using Nanoparticles

Author name: سارة طلال حسين
Supervisor name: جمال مانع علي
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:

تطبيق اساس سيليكا الازالة النفثالين من المياه العادمة في مصافي البترول == Application of Synthesized Silica Based MCM-41 for the Removal of Naphthalene in Petroleum Refinery-Wastew

Author name: خيري رسن كلش
Supervisor name: طالب محمد نايف
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:

تصنيع وتحديد خصائص السيليكا المسامية لنقل المستحضرات الدوائية == Synthesis and Characterization of Mesoporous Silica for Drug Delivery

Author name: حنين فاضل العزاوي
Supervisor name: طالب محمد نايف
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:

تحضير وتوصيف متراكب مطور مادة مغناطيسية /كيتوسان كممتز لازالة الكروم السداسي من الوسط المائي == PREPARATION AND CHARACTERIZATION OF MODIFIED MAGNETIC CHITOSAN NANOCOMPOSITE FOR THE REMOVAL OF CROMIUM (VI) FROM AQUEOUS MEDIUM

Author name: امنة جواد كاظم
Supervisor name: نجاة جمعة صالح | سعد رحيم سلطان
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:

ازالة الملوثات من المحلول المائي بواسطة المادة الميزومسامية المفعلة == REMOVAL OF POLLUTANTS FROM AQUEOUS SOLUTION BY FUNCTIONALIZED MESOPOROUS MATERIAL

Author name: داليا باسل عبد
Supervisor name: انعام اكرم صبري | طالب محمد نايف
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:

دراسة العوامل المؤثرة على عملية تلبيد كلنكر الدولوهايت العراقي لغرض صناعة الحراريات

Author name: مروان غايب الهيتي
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering
University location: Baghdad
Key words:
  • الصخور - العراق - اطروحات الهندسة الكيمياوية

العوامل المؤثرة على ظاهرة تقليل الاعاقة المصاحبة لجريان السوائل بواسطة المضافات البوليمرية والمواد الخافظة للشد السطحي == Effect of Operating Variables On Drag Reduction Phenomenon By Polymers And Surfactants Additives

Author name: ليث مجيد عبود
Supervisor name: issam kamil salih
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:
Abstract: تناول البحث دراسة وتطبيق ظاهرة تقليل الاعاقة لاطالة مسافة تصريف السوائل الساقطة بشكل حر من انبوب افقي. حيث تمت دراسة تاثير ارتفاع ونوع السائل , نوع وتركيز البوليمر , قطر الانبوب وخشونة سطحه, واحدى المواد ذات الفعالية السطحية.تم اجراء الاختبارات العملية | Drag reduction phenomenon has been studied and applied to extend the discharge distance of kerosene, gas oil and tap water falling freely from horizontal tube. The effect of liquid head, type of solvent, polymer characteristics and concentration, pipe diameter and roughness and addition of surfactant were investigated.Experimental tests were performed using apparatus consisting of a reservoir connected to a horizontal tube from which the flux was allowed to fall freely under different heads. The distance traveled horizontally was measured and used to estimate the friction factor (ƒ) and the percentage drag reduction (%DR). The tests were carried out under liquid heads of 140, 165, 190, 215, 240 cm to ensure turbulent flow circumstances, i.e. Re ? 3000.Three types of polymers were tested, viz., polyisobutylene (PIB), xanthan gum (XG) and guar gum (GGM). The activities of these polymers for drag reduction were evaluated at concentrations of 10 - 200 ppm for PIB and 50 - 400 ppm for XG and GGM using three solvents, viz., kerosene, gas oil and tap water. Glass tubes of 3,7,10 and 11mm diameters in addition to carbon steel and stainless steel pipes of 10mm diameter were used to investigate the effect of pipe diameter and roughness.The interactions between polymer and surfactant were investigated using sodium luaryl sulfate (SLS) so that experimental tests were performed with PIB in the absence and presence of (SLS) at different concentrations. The discharge distance and %DR is generally increased with increasing liquid head and additive concentration. However %DR is sometimes reached to a maximum value at a specific concentration termed " critical concentration" beyond which %DR is fallen, the %DR observed with 100ppm of PIB is 44.3% at head equal 140 cm and 56% at head equal 240 cm from stainless steel tube. Moreover, %DR is progressively increased with increasing Reynolds number (Re) at any specific concentration, %DR achieved due to the addition 50ppm of PIB is 20.8% at Re equal 17236 and 45.9% at Re equal 26056 from stainless steel tube.Polyisobutylene has effectively reduced drag with kerosene and gas oil. Its activity seems to be higher with gas oil compared to that with kerosene. The maximum %DR achieved due to the addition 100 ppm of PIB in gas oil and kerosene are 63% & 56% respectively from Stainless steel tube. The activity of SLS for drag reduction with kerosene is evidently lower than that of PIB, and the difference between %DR observed is reduced with increasing concentration. Efficiency of PIB is considerably decreased by adding SLS so that the maximum %DR achieved with their mixture is 40.1%.The polymers XG and GGM are effectively reduced drag when added to tap water. Their activities at any specific operating conditions are decreased according to the sequence of XG ? GGM. The maximum %DR observed with them at 300 ppm are 77% and 48.8% respectively. The values of (%DR) measured with all tested liquids seem consistent with Blasius equation and they are progressively shifted to the direction of Virk asymptote with increasing of polymer concentration. The percent drag reduction is well correlated with Reynolds numbers, (L/D) and polymer concentration according to the relation of the form %DR= a (Re)b (C)d (L/D)k, where a, b, d and k are constants, so that a specific empirical correlation is observed for each polymer.

استخدام المادة النانو مسامية SBA - 15 لازالة الملوث العضوي من المياه الصناعية == A Nanoporous SBA - 15 As Adsorbent For Removal of Organic Pollutants From Wastewater

Author name: رغد عدنان حبش
Supervisor name: انعام اكرم صبري | طالب محمد نايف
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:
Abstract: تم تحضير ماده السليكا النانويه المسامية (SBA - 15) باستخدام (TEOS) كمصدر للسيليكا و(P123) كقوالب ومن ثم اجريت فحوصات عليها منها حيود الاشعة السينية (XRD),المجهر الالكتروني (SEM)،المساحة السطحيه ( (BET وطيف الاشعة تحت الحمراء (FTIR). بعد ذلك تم دراسة سلو | Santa Barbara Amorphous (SBA - 15) nanoporous silica was prepared using Tetraethylorthosilicate TEOS as silica precursor, Pluronic P123 as template, and characterized by means of X - ray diffraction (XRD), scanning electron microscopy (SEM), BET surface area and fourier transform infrared (FTIR) spectroscopy. The adsorption behavior of methylene blue from synthetic wastewater onto mesoporous SBA - 15 was studied. Both batch and continuous systems were studied. Batch experiments were carried out to measure the adsorption as a function of contact time, initial concentration (15 - 110 mg/l), pH (3 - 11) and adsorbent dose (0.1 - 2.3g/l) to specify the optimum operation condition. The equilibrium of the process was achieved within 20 min. Adsorption isotherms were fitted with the Langmuir, Freundlich and Temkin models. The equilibrium data were best represented by the Langmuir isotherm model with higher correlation coefficient R2 value of (0.990). The kinetics of the MB sorption on SBA - 15 were examined by using pseudo - first and pseudo - second order kinetics models. The kinetics analysis manifested that the overall adsorption process was successfully fitted with the pseudo - second - order kinetic model. In continuous studies, the adsorption of methylene blue from synthetic wastewater onto SBA - 15 in fixed bed was investigated and breakthrough data of the dye was determined. This research is run in small scale column with an internal diameter of 0.7 cm and 35 cm height at constant temperature and pH value. The effect of bed height (3, 6, 9 cm), flow rate (0.6, 1.0,1.4 ml/min) and initial MB concentrations (40, 70, 100 mg/l) on breakthrough curves were investigated. It is found that breakthrough time increases with increasing bed height, but decreases with increasing methylene blue inlet concentration and flow rate. Thomas and Yan models were used to determine the kinetic constants and to predict the breakthrough curves. The experimental data showed a better fit to Thomas adsorption model. In order to find out the possibility of reuse SBA - 15, desorption study was also carried out in this investigation. SBA - 15 can be effectively recovered by calcinations and reused fourteenth times in batch system and five times in continuous system without significant loss in removal of methylene blue from aqueous solution. The long reuse life of SBA - 15 makes it an efficient adsorbent for removal of methylene blue from wastewater at high potential for application in industry.

تطبيقات الطرق العددية في التاكل الكلفاني للمعادن المزدوجة == Applications of Numerical Methods In Galvanic Corrosion of Coupled Metals

Author name: بسمة محمد كاظم الشاهر
Supervisor name: جمال مانع علي الربيعي
General topic: Chemical Engineering
Specific topic: Industrial Processes
Degree: Master
University: University of Technology - Department Of Chemical Engineering - Chemical Process Engineering Branch
Language: English
University location: Baghdad
First pages:
Abstract: تم دراسة سلوك تاكل معادن النحاس والكربون الصلب والزنك في تراكيز مختلفة من حامض الهيدروكلوريكHCl) ) (0.025، 0.05 و0.075 مولاري ) عند درجات حرارة مختلفة (30، 40 و50 درجة مئوية) باستخدام القياسات الكهروكيميائية (Electrochemical Measurements) في حالة المعا | The corrosion behaviors of metals Copper, Carbon Steel and Zinc in a different concentrations of HCl acid (0.025, 0.05 and 0.075M) at different temperatures (30, 40 and 50°C) were investigated using electrochemical measurements in couple and single state.The galvanic behaviors of coupled metals (Cu - Fe),( Cu - Zn) and (Fe - Zn)were studied using Zero Resistance Ammeter (ZRA) technique, it has been used to measure the galvanic current (Ig) and galvanic potential (Eg) with time. The galvanic corrosion cells for all couples have equal areas of anode and cathode (2×2cm).The galvanic current density (ig) is increased with increasing solution concentration and temperature. The galvanic potential (Eg) is shifted to less negative with increasing solution concentration and temperature and it is close to the corrosion potential of the anode in the couple conditions.The potentiostatic polarization behavior of single three metals (Copper, Carbon Steel and Zinc) in different concentrations of dilute HCl acid (0.025, 0.05 and 0.075M) at temperature (40°C) is found under activation control. The corrosion current density is increases with increasing solution concentration and gives the following arrangement of metals : Cu> Fe > Zn A numerical analysis of galvanic corrosion was presented. The analysis was based on three numerical methods as the boundary element method (BEM), the finite element method (FEM) and the finite difference method (FDM).The potential and current density distributions on the galvanic elements are described by the Laplace equation. The Laplace equation was solved numerically, to determine the potential, current density, and corrosion caused by the galvanic cell using designed computer programs in MATLAB R2014a. The experimentally determined polarization curves have been used in order to define the nonlinear boundary conditions. This boundary value problem has been solved using Newton - Raphson iterative numerical procedure. For the three couple systems (Cu - Fe, Fe - Zn and Cu - Zn), the results obtained for galvanic potential and current density, using the numerical methods (BEM, FEM and FDM) with the overall deviations are 6.689, 10.818 and 18.846 respectively for galvanic current density and 0.631, 1.210 and 1.787 respectively for galvanic potential. From these results it can conclude that the galvanic current density and galvanic potential distribution calculated from the BEM model was in good agreement with the experimental measurements. These are because the main advantages of the BEM over the Finite Element Method (FEM) and the finite difference method (FDM) are high accuracy, discretization on the boundary only which results in a very small number of unknowns, easy dealing with non - regular boundaries and openings that only the domain boundary of interest is required to be discrete, also BEM needs fewer equations and a smaller matrix size than FEM and can solve both finite and infinite domain problems.