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تحضير وتشخيص بعض المركبات الحلقية غير المتجانسة الجديدة المشتقة من الجالكون واستخدامه بعضها كمضادات للاكسدة == Synthesis and characterization of some new heterocyclic compounds derived from chalcone and used as antioxidants

Author name: ميس كامل كطافة السراجي
Supervisor name: عباس فاضل عباس | خنساء عبد الرزاق
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:

تحضير ودراسة الخواص الحرارية والضوئية لبعض الراتنجات الفينولية واستخدامها كمصلبات لراتنج الايبوكسي == Synthesis and Study of Thermal and Optical Properties of some Phenolic Resin and Use it as Hardener for Epoxy Resin

Author name: فهـد معـروف صالح الشاوي
Supervisor name: وداد صالح الفياض | خنساء عبد الرزاق الاسدي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:

تحضير وتشخيص ودراسة الفعالية البيولوجية لبعض قواعد شف المشتقة من عقاقير السلفا وبلمرتها ودراسة خصائصها الحرارية == Synthesis, Characterization and Study of the Biological Activity of Some Schiff Base Derived From Sulfa Drug , Its Polymerization and Study Thermal Properties

Author name: حيدر حسين عبد علي
Supervisor name: بشرى كامل السلمي | محمد احمد عبد
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:

تحضير وتشخيص بعض مركبات بيتا - امينو كاربونيل الجديدة وبعض معقداتها مع النحاس الثنائي ودراسة العلاقة الكمية بين فعاليتها الحيوية والتركيب == Preparation and Characterization of some new ?-amino Carbonyl Compounds and some of their Cu(II) Complexes and Quantity Structure Activity Relationship study

Author name: حنان فؤاد مزعل الشمسي
Supervisor name: هانوي كمال العامود | حياة حمزة عباس العبد العظيم
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:

دراسة تاثير نبات الكراث Allium Porrium L على مستوى السكر والكوليسترول في دم الارانب الطبيعية والمصابة بفرط السكر المحدث بوساطة الالوكسان == study the effect of allium porrium l. on blood glucose and cholesterol levels in normal and hyperglycemic rabbits induced by alloxan

Author name: زينب شاكر عبد الله علي
Supervisor name: عيسى عبد عبد الحسن
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:

تحضير وتشخيص ودراسة بعض مركبات السيلينيوم العضوية الجديدة الحاوية على النتروجين == preparation characterization and study of some new orange - selenium compounds containing netrogen

Author name: علي جميل حميد الحمد
Supervisor name: لينا زكي يوسف
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:

دراسة الطيف الرنين الالكتروني البرمي لبعض البلورات السائلة

Author name: عبد الرزاق محمد رؤوف
General topic: Chemistry
Specific topic: Organic Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
University location: Basrah
Key words:
  • البلورات السائلة

التوصيف الجزيئي للمستضد السرطاني CA125 في اورام المبايض الحميدة والخبيثة باستخدام تقنية الاختبار المناعي الاشعاعي المتري == Molecular characterization of CA125 in Benign and Malignant Ovarian Tumors Using Immunoradiomatric Assay Technique

Author name: ماجد حسن قربون
Supervisor name: SAMI AL-MUDHAFFER
General topic: Chemistry
Specific topic: Biochemistry
Degree: Doctorate
University: University Of Basrah - College Of Science - Chemistry Department
Language: English
University location: Basrah
First pages:

تحضير وتشخيص ودراسة الفعالية البايولوجية والخواص الكهروكيميائية لبعض مركبات السلفانايترون الجديدة == Synthesis, Characterization, Biological activity and Electrochemical Study of Some New Sulfa-Nitrone Compounds

Author name: هدى صالح عبود
Supervisor name: Nesreen N. Majeed | Anis Al-najar
General topic: Chemistry
Specific topic: Chemistry
Degree: Doctorate
University: University Of Basrah - College Of Science - Chemistry Department
Language: English
University location: Basrah

تحضير وتشخيص بعض المركبات الحاوية على بعض العناصر اللاعضوية ودراسة استخدامها في تقسية الايبوكسي وازالة بعض الايونات الثقيلة == Preparation and Characterization of some compounds containing inorganic elements , using them as epoxy hardener and removal of heavy ions

Author name: هدى مصطفي ناصر
Supervisor name: تحسين علي صاكي | مجيد يعقوب اللعيبي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

ثايزين وبعض معقداتها وتقييم 3,1تحضير وتشخيص بعض مشتقات خاصية امتزاز هذه المشتقات في معالجة المياه == Synthesis and Characterization of Some New 1,3 -Thiazines and their Complexes and Evaluation of their Adsorption Capacity for Water Remediation

Author name: ندى قاسم جبر
Supervisor name: علي عبد الرزاق عبد الواحد | علي جميل حميد
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

نظام الحقن الجراني والتالق الكيميائي لتقدير بيروكسيد اليدروجين باستخدام كاشف اليمينول والموبايل والموبايل كمكشاف جديد == Flow Injection Chemiluminescence System For Determination of H2O2 by Using Luminol as Reagent and Mobile-Phone as New Detector

Author name: مصطفى عبد الكاظم حسين علي
Supervisor name: كامل حسين علوان السوداني
General topic: Chemistry
Specific topic: Analytical Biochemistry
Degree: Doctorate
University: University Of Basrah - College Of Science - Chemistry Department
Language: English
University location: Basrah

استخدام البوليمرات المحضرة والمشتقة من مخلفات بولي ترفثالات الاثلين في ازالة بعض المبيدات من المياه == Using of some prepared polymers derived from poly(ethylene terephthalate) waste to remove some pesticides from water

Author name: مريم صباح عبد الرحمن
Supervisor name: حسن ثامر عبد الصاحب | صلاح شاكر هاشم
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: English
University location: Basrah

تحضير وبلمرة بعض مونيمرات الفيروسين العضوية واستعمال الفيروسين كمعجل للمونيمرات الميثااكريلاتيه == Synthesis and Polymerization of Some Organic Ferrocene and Use the Ferrocene as Accelerator for Polymerization of Methacrylate Monomers

Author name: علاء كامل حنون نزال الخالدي
Supervisor name: هادي سلمان اللامي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: English
University location: Basrah

تحضير، تشخيص ودراسة الفعالية البكتيرية لبعض مركبات الثايازول وقواعد شف والازتيدينون الجديدة بوساطة المايكرويف == Microwave Assisted Synthesis, Characterization and Antibacterial Study of Some New Thiazole, Schiff Base and Azetidinone Compounds

Author name: زكي عصمان ناصر الشمخاني
Supervisor name: حنان عبد الجليل راضي الهزام
General topic: Chemistry
Specific topic: Chemistry
Degree: Doctorate
University: University Of Basrah - College Of Science - Chemistry Department
Language: English
University location: Basrah

تحضير وتشخيص ودراسة تحليلية وكهربائية لمعقدات بعض ليكاندات قواعد شف مع ايونات Co(II) Ni(IIو Cu(II) == Syntheses, characterization ,analytical and electrochemical studies of the complexes of some new Schiff base with Co(II), Cu(II) and Ni(II)ions.

Author name: بيداء حيران جعاز
Supervisor name: هناء حميد حداد | علي عبد الامام الرياحي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

تقييم التاثير المنخفض لفرط سكر الدم لمستخلصات وريقات نخيل القنطار ضد مرض السكر == Evaluation of Hypoglycemic effect of Phoenix dactylifera Ganthar Leaflets Extracts Against Diabetes Dise

Author name: رنين سالم سوادي
Supervisor name: عباس دواس مطر المالكي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

تحضير و تشخيص و دراسة فيزيوكيميائية و حيوية لبعض معقدات الروثينيوم II والبلاتين مع بعض القواعد النتروجينية == Synthesis, Characterization Physicochemical and Biological studies of some Ruthenium(II) and Platinum(II) Complexes with some of nitrogenic bases

Author name: سهى يوسف نصار
Supervisor name: محمد جاسم بدر الاسدي | اقبال جاسم بدر الاسدي
General topic: Chemistry
Specific topic: Inorganic Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

تحضير وتشخيص ودراسة الفعالية البيولوجية لبعض المركبات العضوية والعضوية لفلزية الجديدة المتضمنة النتروجين

Author name: زينب كاظم الخزرجي
Supervisor name: بشرى كامل السلمي | عادل علي الفريجي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

تحضير وتشخيص ودراسة طيفية وكهربائية لبعض معقدات الفثالوسيانين واشباهها وتشويبها بمشوبات عضوية ولاعضوية == Synthesis, Spectroscopic and electriecal studies for some Phthalocyaninen and Semiphthalocyanine complex and their doping with organic and inorganic dopants

Author name: ايات جودت كاظم مجيد
Supervisor name: نزار عبد الامير حسين
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

تحضير وتشخيص ودراسة الفعالية البايولوجية وكمضادات اكسدة لبعض مشتقات الغابابنتين ومعقداتها مع [Zn(II), Cu(II)] == Synthesis, Characterization, Biological Activities and Antioxidant Study of Gabapentin Derivatives and their complexes with [Cu(II), Zn(II)]

Author name: اسامة حسن سالم البدران
Supervisor name: ظافر محمد حسين المظف | لي حسين الموالي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah

تحضير وتشخيص مثبطات تاكل جديدة من اعادة تدوير بولي اثلين ترفثاليت وتقييم كفاءتها في تثبيط تاكل الصلب الكربوني في الوسط الحامضي == Preparation and Characterization of New Corrosion Inhibitors from Polyethylene Terphthalate (PET) and Study its efficientcy As to Inhibit the Corrosion of Carbon Steel in Acidic Media

Author name: منتظر فريد الاسدي
Supervisor name: مؤيد نعيم خلف
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:
Abstract: The research included synthesis ,characterization and evaluation of new corrosion inhibitors(bis(2 - hydroxy ethyl) thioterphthalte and bis(2 - hydroxyethyl)terephthalate from recycled waste polyethylene terephthalate . The best percent of the two corrosion inhibitors were reached after many experiments, which included study many factors like temperature, catalyst , the equivalent weight of reactants and others. The synthesized corrosion inhibitors were characterized by FTIR spectroscopy . The two inhibitors were evaluated as corrosion inhibitors using sulfuric acid as corrosion media for carbon steel( carbon steel C1010) . The factors effect on the rate of corrosion like temperature , concentration of inhibitor were studied by the electrochemical technique using the Tafel plot. The obtained results at temperatures range ( 298, 308,318,328 K) were used to calculate many factors that determined the efficiency of the inhibitor like corrosion rate , charge transfer resistance and inhibitor efficiency. it was observed that the corrosion rate and charge transfer of the carbon steel for the inhibitors increases with increase of temperature and decreases with increase of the inhibitor concentration in the same temperature. The Results showed that both inhibitors had very high inhibition in reducing the corrosion rate . The inhibition efficiency reached (96%) for the bis(2 - hydroxy ethyl) thioterphthalate for the 24ppm and (91%) for the bis (2 - hydroxy ethyl) terephthalate for the 25ppm .Many thermodynamics functions was calculated ,activation energy a ,entropy S , enthalpy  and free energy G during the different experiment conditions ,which was indicated of the corrosion inhibition efficiency and the type of the inhibition. The obtained results showed that the two inhibitors were very efficient to reduce the corrosion rate in the acidic media and from the G data the type of adsorption was chemical because the value of Gads was higher than (20 KJ/mol) .

تحضير وتشخيص وتقييم بعض معقدات قواعد شف لايوني النحاس والموليبدينوم كمثبطات تاكل لسبيكة حديد الصلب الكربوني في الوسط الحامضي == Preparation, Characterization and Evaluation of Some Schiff Base’s Complexes of Copper and Molybdenum Ions as Corrosion Inhibitors for Carbon Steel Alloy in Acidic Medium

Author name: محمد علي مهدي الحلفي
Supervisor name: زكي ناصر كاظم | هادي زيارة محمد
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:
Abstract: In this study, two types of Schiff base were prepared as ligands L1, L2, by reaction of an equal number of moles of tris(hydroxymethyl) methyl amine with salysildehyde and vanillin in a methanolL1 : ((E) - 2 - ((2 - hydroxybenzylidene) amino) - 2 - (hydroxymethyl) propane - 1,3 - diol) L2 : ((E) - 2 - ((4 - hydroxy - 3 - methoxybenzylidene) amino) - 2 - (hydroxymethyl) propane - 1,3 - diol).The Cu(II) and Mo(VI) complexes were prepared to produce the : - A1 : tetrakis(μ3 - 2 - {[1,1 - bis(hydroxymethyl) - 2 - oxidoethyl] iminomethyl} - phenolato) tetrakis [aqua copper(II)].A2 : tetrakis(μ3 - 2 - {[1,1 - bis(hydroxymethyl) - 2 - oxidoethyl] iminomethyl} - 2 - meth - oxy} - phenolato) tetrakis [aqua copper(II)].B1 : (E) - 2 - methyl - 2 - ((2 - ((methyl(l1 - oxidanyl) dioxomolybdenio) oxy) benzylidene) amino) propane - 1,3 - diol).B2 : (E) - 2 - ((4 - hydroxy - 3 - ((methyl(l1 - oxidanyl) dioxomolybdenio) (methylene) - l4 - oxidanyl) benzylidene) amino) - 2 - methyl) propane - 1,3 - diol).The ligands and complexes were characterized by Fouries transformer infrared FTIR, UV and NMR techniques.All these techniques insisted that the ligands and their complexes were prepared successfully.On the other hand, the four complexes A1, B1, A2 and B2 were evaluated as corrosion inhibitors against a corrosive environment of 0.1M of hydrochloric acid at constant temperature of 25°C and different concentration for each one of the above complexesIIrange (10 - 50) ppm and it has been found that the efficiency of inhibition at a temperature 25℃ are not highly efficient, the KI was added in order to increase the efficiency of these inhibitors values to these inhibitors.The inhibition efficiency for all inhibitors was increased in presence of KI compared with the absence of it.On the other hand, the complexes of copper i.e., A1 and A2 have higher efficiency than molybdenum complexes i.e. (B1 and B2) this can be attributed to the ability of copper ion (II) to donate the electron density to the ligand by back donation competence these behaviour compared with molybdenum ion (VI) that has not the ability that present in copper ion, Also studied the effect of concentration of the inhibitor prepared in other temperatures change separately and these grades are within the range (35 - 55) ℃ has been observed that efficiency does not increase either the existence of KI with the inhibitor, or without, but the decreasing efficiency with increasing temperature, means that the inhibitor adsorbed physically on carbon steel alloy.The functions thermodynamic adsorption such as free energy, enthalpy and entropy were studies depending on the adsorbent layer θ on the surface of the carbon steel alloy. The data was shown all the complexes are subject to model for Langmuir adsorption was shows the free energy negative values means that the interaction is spontaneous and notes total increasing of the temperature less than the negative value of the free energy leading to towards the is non - spontaneous. The negative values of enthalpy means that the interaction is exothermic, the negative value of the entropy of adsorption ΔSads and gradually moving toward positive values with a high temperature means that the random was less in high temperature. Also the kinetics of corrosion in the absence and present of the inhibitor was studied with KI in (0.1) M HCl. The activation energy and other thermodynamic function such as enthalpy and entropy and free energy was shown that the higher activation energy in presence inhibitor and it was higher in presence of KI with inhibitor. This is an indication that the interaction of corrosion is small in the presence of these inhibitors.

تحضير مدعم بالاشعة المايكروية ودراسة الفعالية البكتيرية لقواعد شف المشتقة من 4 - كلوروبنزالديهايد مع بعض الاحماض الامينية وتحضير بعض معقداتها == Microwave - Assisted Synthesis and antibacterial activity of som Schiff bases derived from 4 - chlorobenzaldehyde with some amino acids and their complexes

Author name: رغد كاطع عبد الصاحب
Supervisor name: قحطان عبد عسكر | بشرى كامل جدوع
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:
Abstract: This thesis is concerned with the synthesis of some Schiff bases derived from condensation of selected α - amino acid ( glycine , alanine , phenyl alanine , valine, and threonine ) with 4 - chlorobenzaldehyde by using microwave irradiation as shown in the general equation : Some complexs derived from these Schiff bases with some transition metal (Co++, Cd++, Ni++, Zn++, Cu++) tow types of complexes were obtained , the first kind of complexes suggested to be which have octahedral structure possess and the proposedfollowing structure : While the second kind of complexes which have tetraheadral structure possess following structure : All ligands and their complexes have been characterized by IR, CHN elemented analysis thermal gravimetry analysis(Tg) .The H1NMR studies were done by DMSO as solvent . The mass technique was used to record the mass spectra which showed [M+] ions at the proposed [M.W] confirming the expected molecular weights .The analytical data showed that the Schiff bases can act as bidentate Ligand using the N - isomethinc and O - carboxylate with ratio 2 : 1 (L : M) while complex show that the ratio was 3 : 1 (L : M) and have octahedral structure possess the proposed following structure : The low molar conductance of the complexes indicate that they are non - electrolyte and neutral .The antimcroble activity of Schiff bases and their complexes were tested against two types of bacteria (Staphylococcus aureus (+) , Aeromonas hydrophila ( - ) ). and the results showed that some of them have an excellent or moderate antibacterial activity

استخلاص وعزل بعض المركبات الفعالة بايولوجيا من جمار النخيل Phoenix dactylifera == Extraction and Isolation Some Active Biological Compounds From (Phoenix dactylifera)

Author name: وصال عبد الرحمن سالم الثامري
Supervisor name: اقبال جاسم بدر | هناء كاظم موسى
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University Of Basrah - College Of Science - Chemistry Department
Language: Arabic
University location: Basrah
First pages:
Abstract: It is notable that Iraq characterized by the availability of palms trees , according to 2012 statistics it has been considered as the fifth largest country in production of dates in the world (Wikipedia), and because of the rareness study about the palm it almost non - exist in Iraq , therefore it has been proposed this study in order to find out the medical uses of the Jummar .The study has included preparation of five extracts which they are aqueous ,70% alcoholic , glycosidic , alkolids and flavonoids .In addition , the isolated oil and makes some chemical and physical detections such as solubility.Moreover , it included knowledge of content for this extracts and identify the number of components in each extract and diagnose the chemical identity using several techniques such as "Thin layer and Colum" chromatography ," FTIR , U.V - Visible" spectroscopy.It has also been studied the effect of the glycosidic , alkolids , flavonoids and oil extracts on the level of blood sugar in normal rabbits and the rabbits suffering from hyperglycemia which induced by alloxan ,in addition to the effect of the pill lower the blood sugar and the mixture from the pill with alkloidic extract , beside the mixture of the pill with oil extracts.Furthermore, the test giving a potion (dosage - dose) of 500mg/Kg which is had reduced the blood glucose level for 24h with significant difference p> 0.001 , the isolated oil was less efficient with significant difference p> 0.001 .The cytotoxicity test was also conducted by using In vivo method on human blood does not affected by isolated compounds from Jummar and oil isolated oil , and it safe and non - toxic.The effect of above extracts was studied on the growth of some kind of positive Gram Staphylococcus aureus , and negative Gram bacteria Aeromonas hydrophila using Agar diffusion method , the flavonoid extract showed the high test 16mm inhibition zone compared with alkaloid extract which showed 12mm inhibition zone for negative Gram bacteria Aeromonas hydrophila.The effectiveness of isolated compounds and oil isolated were estimated as antioxidants and compare them with Butyrated hydroxyl toluene (BHT) which appeared that flavonoids extract has a higher effective antioxidant.The interference of isolated compounds from palms jummar and isolated oil with DNA has been studied by tracking the change in the concentration of the isolated compounds after mixing with DNA in the various time and by tracking the change of the UV spectroscopy. Finally , it has been also tracking the change of the concentration of DNA by using the Electrophoresis Technology and UV photographic technology and both Technologies showed the interference between the isolated compounds and the DNA.Also the glycosidic extracts was studied on the growing of cancer cells Rhabdomysarcoma , and seemed clear inhibition at concentration (10mg/ml) in (72) hours and inhibition ratio was about (37.26%).
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