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استخلاص وعزل وتشخيص المركبات متعددة الفينول اكاسيتين كلايكوسيدات من بذور نبات الحلفا السبخبة ودراسة الفعالية الحيوية للمستخلص كمضاد فطري وبكتيري == Extraction, Isolation and identification of poly phenols compounds (acacetin glycosides) from Cladium Mariscus seeds and study of their biological activity of extract as antifungal and antibacterial agent

Author name: رحاب حاتم بريج الشمري
Supervisor name: حسام محمد كريدي | محمد تركي خثي
General topic: Chemistry
Specific topic: Analytical Biochemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: English
University location: Dhi Qar

تحضير وتشخيص ودراسة بايولوجية لمشتقات جديدة من 4,2,1 - ترايازول ومعقداتها مع بعض العناصر الانتقالية == Preparation, Characterization and biological study of some new 1,2,4 - Triazole derivatives and theirs complexes with some transition metals.

Author name: احمد كامل عجيل الزيدي
Supervisor name: ابراهيم عبود فليفل
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: Arabic
University location: Dhi Qar
Abstract: he work listed by this thesis covers the preparation and characterization ofsome new derivatives of 1,2,4- Triazole as ligands which are : | 1-N : ( 2-ethyl-5-{[(3-phenyl-5-sulfanyl-4H-1,2,4-triazol-4-yl)imino]methyl}benzene-1,4-diol). (L1)2-4-({2-[(4-methylphenyl)amino]ethylidene}amino)-5-phenyl-4H-1,2,4-triazole-3-thiol (L2)3-5-methyl-4-{[1-(5-methylfuran-2-yl)ethylidene]amino}-4H-1,2,4-triazole-3-thiol (L3) | Those ligands were used to prepare some complexes such as L1,L2,L3with the chlorides of transition metal(FeCl3.6H2O,COCl3. 6H2O,CrCl3.6H2O,CuCl2.6H2O,NiCl2.6H2O)To characterize the structure of prepared ligands and their complexes, | elemental analysis (C.H.N),Infrared Spectroscopy (IR), NuclearMagnetic Resonance Spectroscopy(1H-NMR),Mass Spectra,Magneticsensitivity and Molar conductivity techniques were applied . The resultsshowed that ; | 1- The complexes of [Fe(III) , Co(III) , Cr(III)] for all ligands haveshown octahedral configuration. | 2- Complexes of [Ni(II) , Cu(II)] with all ligands have shown square | planer configuration.Testing the biological activity for ligands and their complexes by using spread method and measurement inhibition zone by using (DMSO) as asolvent showed a positivity results; By the appear laeg inhibition zonesagainst E-coli and S. aureas species of bacteria.

تحضير وتشخيص ودراسة بايولوجية لبعض مركبات ثنائية الازو الجديدة ومعقداتها واستخدامها كوثبطات لتاكل سبيكة الفولار الكاربوني في الوسط الحامضي == Synthesis,Characterization and Biological activity Study of Some Bis - Azo Dyes and their Complexes and the use of Bis - Azo dyes as Corrosion Inhibitors for Low Carbon - Steel in acidic media

Author name: اسراء عبد الكاظم جاسم الشمري
Supervisor name: ساجد حسن كسار | حسام محمد كريدي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: Arabic
University location: Dhi Qar
Abstract: As it used for dyes (A1,A3) P-Phenylenediamine ,while using for dyes (A2,A4) O Phenylenediamine. | here is X for dyes (A1,A2) 3-ethoxy salicylaldehyde ,while representing for | dyes 3-methoxy salicylaldehyde. | he prepared copmpounds were identified by FT-IR spectroscopy, CHN analysis, 1H-NMR spectroscopy and GC-Mass spectroscopy.Also, determination of melting pointsWhere,XIn the recent study, four azo dyes compounds were prepared (A1-A4) and tested as The inhibition efficiency of the synthesized compounds was studied , using | weight loss method in acidic solution by corrosion rate determination for | carbon steel without and with different concentratins | ) 1 , 5 , 1 , 5 ( M | of inhibitor at different immersion times (1-5) hrs ,303K and static condition | .The inhibition efficiency of synthesized compounds was calculated ,the | optimum concentration ( 5 M ) and immersion time (5 hrs) were | determined at the same conditions.The compounds have agood corrosion | inhibition with efficiency percentage of (86.47-88.26%) for azo dyes. | The effect of temperature variation on the corrosion rate for different | concentrations (1 -5 M) of the prepared compounds was studied | by using weight loss method at four temperature degrees (303, 313,323 and | 333)K and (1-5) hrs. | The experimental results of temperature effect indicated the following : | 1-The rate of corrosion inhibitors increased with the rise of temperature, while | the corrosion rate decreased with increasing of inhibitor concentration at the | certain temperature.For example ,the corrosion rate for carbon steel in the | presence of A2 inhibitor increased from 39.22mpy at 303K to 464.75mpy at | 333K.while the corrosion rate decreased from 70.50mpy at concentration of | 1 M to 39.22 mpy at concentration of 5 M at constant | temperature of 303K. | 2-All inhibitors had high inhibition efficiency in reducing the corrosion rate.The | inhibition efficiency was decreased by increasing the temperature ,for example | inhibition efficiency for A2 inhibitor was decreased from 88.26% at 303K to | 85.44% at 333K. | 3-The adsorption of the molecules on the metal surface obey Langmuir | isotherm.The adsorption constant and free energy of adsorption were | calculated for the studied inhibitors.The results showed that the adsorption | constants were decreased with increasing the temperature and the negative | value of free energy indicated that the adsorption process is spontaneous. | 4-Thermodynamic functions H and S and the activation energy Ea were | determined.The results indicated that the activation energy for acidic solution | without inhibitor (16.21 KJmol-1 )was less than of the activation energy value | with the presence of inhibitor s, (17.08-31.07 KJmol-1 ) for azo dyes .The | positive value of enthalpy indicated that the metal dissolution process is | endothermic , while the negative value of entropy reflected the reducing in the | entropy value and formation stable layer on the metal surface. | Electrochemical method (Tafel plot) was used to evaluate the inhibition | efficiency for the azo compounds using carbon steel corrosion in 0.5M HCl | solution. The percentages of inhibition efficiency were 86.84%, 93.68%, 86.70 | and 93.06% for the inhibitors A1, A2, A3 and A4, respectively, at 303K and | concentration of 5 x 10-3M. Tafel plot results indicated that the prepared azo | dyes compounds are the doublet inhibitors type. | Studying of the growth inhibition against three types of pathogenic bacteria | namely for some pigments lecture(A1,A2) and their Nickel(II) complexes by | using diffusion method and measurement inhibition zone by using (DMSO) as a | solvent , using in this study three types from bacterial two its Gram negative | bacterial strains, Escherichia coli, Pseudomonas Aeruginosa and the other is Gram positive bacterial strains , Staphylococcus aureus , We notice that the biological activity against this bacterial showed a positivity results. | Ciprofloxacin were used as standard bactericide and compared inhibition this | bacterial with Ciprofloxacin.corrosion inhibitors in acidic medium ,0.5M HCl. These compounds have general chemical structure :

تحضير وتشخيص ودراسة الفعالية البايولوجية لمشتقات جديدة من 4.3.1 اوكسادايازول ومعقداتها مع بعض العناصر الانتقالية == Preparation , characterization and biological activity of a new1,3,4 - oxadiazole derivatives and some of their transition metal complexes

Author name: ايمان حسين شويل التميمي
Supervisor name: ابراهيم عبود فليفل | احمد حسن محمد
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: Arabic
University location: Dhi Qar
Abstract: The work described in this thesis is mainly concerned with preparation and characterization of three ligands (L1-L3) derived from 1,3,4-Oxadiazole .The study deals with reaction of these ligands with transition metal salts as (CrCl3.6H2O , CoCl2.6H2O , NiCl2.6H2O , CuCl2.2H2O) .The ligands and their complexes were characterized by the elemental analysis (C,H,N), Infrared spectroscopy (IR) , Proton Nuclear Magnetic Resonance Spectroscopy (1HNMR), Mass spectra and molar conductivity. However, the ligands and some of their were studied by using hyperchem7.5 program in order to know their geometry and proving their shapes and hypridizaion which were notice the chromium complexes is octahedral (oh), the hypridization is d2sp3 with the three ligands while the shapes of the complexes (cobalt(II), Nickel(II), Cupper (II) ) is four coor-dinated is square planar and the hypridizaion is sp3. | Antibacterial activity was carried out against Escherichia coli, Staphylococcus aureus, Streptococcus pyogenes and Klepsiella pneumonia, and with test compounds at four concentrations of (5, 2.5, 1.25, 0.625mg/ml). Azithromycin and Cefoaxime were the standard drugs utilize. Some of these compounds showed good efficacy, while others ranged from medium to small. | The hemolysis activity of the compounds was tested at different concentrations (5, 2.5, 1.25, 0.625mg/ml) and the results showed high percentage of hemolysis for all these compounds and these gave a conclusion about the contraindication use of these compounds in vivo .

تحضير وتشخيص قواعد شف ومعقداتها المشتقة من 4 - امينوانتيبايرين واستخدامها في استخلاص ايون النيكل الثنائي == Preparation and Characterization of Schiff Bases and their Complexes Derived from 4 - Aminoantipyrine and using them in the Extraction of Nickel (II) Ion

Author name: اسراء جرجيس نعمة
Supervisor name: ساهر عبد الرضا علي | حيدر عباس مهدي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: Arabic
University location: Dhi Qar
Abstract: The study includs the preparation and charazchtion of three new compounds of the schiff bases are : | 1- L1 is prepared from the condensation of 4-amino antipyrine with Penzaal acetone . | 4,4'-((1Z,1'E)-(1-phenylbutdiylidene)bis(azanylylidene))bis (1,5-dimethyl-2-phenyl-1Hpyrazol-(2H)-one)3 | 2- L2 is prepared from the condensation of4-amino antipyrine with Asetayl acetone | 4,4'-((1Z,1'E)-pentane-2,4-diylidenebis(azanylylidene))bis(1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)- one | 3- L3 is prepared from the condensation 4-amino antipyrine with Slsldehid as a first step then it is is reactance output with 3.4-di amino toluene . | 2,2'-((1Z,1'E)-( (3E,3'E)-3,3'((4-methyl-1,2-phenylene)bis(azanylylidene)) bis(1,5-dimethyl-2-phenyl-2,3-dihydro-1H-pyrazole-4-yl-3- ylidene))bis(azanylyidene))bis(methanylylidene))diphenol | The ligands were characterized by using Elemental Analysis (C.H.N), Infrared Spectroscopy (FT-IR) ,Uv-visible Spectroscopy , Nuclear Magnetic Resonance Spectroscopy (1H-NMR) , Mass Spectra . It is appeared that prepearing ligands are tetra chelatingagents kind (N2O2) for the ligands L1 and L2 and kind (N4) for the ligand L3. The complexed are prepeared from reaction the prepearing ligands with some transitional elements (Ni+2 , Co+2 , Cu+2) and the ligends and their complexes were characterized by methods of spectral analysis,Uv-visible Spectroscopy,Infrared Spectroscopy (FT-IR) , Mass Spectra and the Molar Electrical Conductivity .And from the result that we know the complexes are octahedral and their general formula [M(L) Cl2] , whereas M = Ni+2 , Co+2, Cu+2 . The study includs an extraction of nickel(II) ion from its aqueous solutions using solvent extraction technique by employing the reagent L3. The optimum extraction conditions are studied to obtain a better distribution ratio of values for (D) to reach the best percent extrected (%E) to extract nickel (II) ion . It is noted that the best values of distribution ratio (D) and the best percent extrected (% E) extracting nickel ion duo with the reagent L3 at the time of shake (15) minutes .The best extraction to nickel(II) ion with reagent L3 at temperature (25C°). As it turns out from this study that the best acidic function nickel(II) ion extraction in the aqueous phase with reagent L3 in the organic phase | when the (PH=9),also the study shows that the best values of distribution ratio (D) and the percent extrected (% E) for nickel(II) ion extraction when its constriction was (120 μg/ml) | (4.5×10-4 M ).The reagent L3 concentration (1× 10-4 M) . Chloroform was the best organic solvent for an extraction process for nickel(II) ion with reagent L3.The reagent L3 also is used for extraction Ni+2 from water of the Euphrates River City of Nasiriyah and the distribution ratio (D) =4.81 and the precent of extrected =%82 as it becomes out the reagent has high efficiency for extrected from the sample .

تحضير وتشخيص بعض مركبات النايترون الجديدة ودراسة الفعالية البايولوجية لها == SYNTHESIS And characterization OF Some new Nitrones Compound and The study of biological effectiveness

Author name: زهراء حميد كامل
Supervisor name: ماجد حمود مزيعل
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: Arabic
University location: Dhi Qar
Abstract: This study was included the preparation of a series of compounds heterogeneous Nitrones. Novel compounds were resulting from the reaction between azo compounds and hydroxylamine compounds through several steps. | the first step was synthesis of a new azo compounds for 2-aminopyridine includes (2a, 2b, 2c, 2d) by configuration the diazonium salt, which in turn enters the reaction of duplication with these aldehydes (2-nitro benzaldehyde, 4-dimethylamino benzaldehyde, 4-chloro benzaldehyde and 4-hydroxy benzaldehyde) respectively. | The second step was included the preparation of hydroxylamine compounds, (N-phenyl hydroxylamine and N-p-toluidine hydroxylamine) were reduced depending on the methods published in the literature. | The third step included the reaction between N-phenyl hydroxyl amine and azo compounds to gave nitrones compounds first set (3a, 3b, 3c, 3d) respectively. | Also we prepare nitrones compounds by the reaction between azo compounds with N-p-toluidine hydroxylamine to give Nitrones compounds second set (3e, 3f, 3g, 3h). | It has been identified the both novel azo-aldehydes and nitrones compounds by using infrared spectroscopy (FT-IR), spectrum NMR proton (1H-NMR), spectrum NMR carbon (13C-NMR) and mass spectrometry (Mass Spectra ) as well as we measured the Melting point for the preparing compounds. | We also Study the effectiveness of biological compounds of the prepared compounds inhibited the growth of some bacteria positive and negative gram, it has shown some compounds to be effective in killing or inhibition of these germs. | next table shows the compounds prepared in this study.

تحضير وتشخيص بعض مركبات N - Oxide جديدة ودراسة فعاليتها الحيوية == Synthesis and characterization of some novel N - Oxides and Study their Biological activities

Author name: نور عبد الخضر سلمان الاميري
Supervisor name: ماجد حمود الصافي | محمد عجه عوده
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: Arabic
University location: Dhi Qar
Abstract: In this study, we prepared a series of nitrones compounds resulting from the interaction of azo dyes prepared which contain Carbonyl edge with hydroxylamine compound . | It was prepared a series compounds of azo dyes (A1, A2, A4, A5) have been prepared by the reaction between 2- amino pyrimidine with diazonium salts which contain benzaldehyde derivatives(4-hydroxy benzaldehyde, 4- chloro benzaldehyde, 4-dimethylamino benzaldeyde, 2- nitro benzaldehde). While the compound A3 was prepared by the reaction between 6-amino-2-mercaptopyrimidin-4-ol with 4-hydroxy benzaldehyde.It was also prepared two groups of Nitrones, the first | group includes the compounds (B1, B2, B3, B4, B5) resulting by the reaction between azo dyes prepared (A4, A2, A5, A1, A3) respectively with N-phenyl hydroxylamine. | On the other hand the second group includes the compounds( C1, C2, C3) resulting by the reaction between azo dyes (A4, A2, A1) respectively with NParatolyl hydroxyl amine Those compounds have been confirmed the authenticity | of the molecular structures of the compounds prepared | using the TLC, infrared spectroscopy and 1H-NMR | spectrum and 13C-NMR spectrum. | It has also been study the toxicity by the calculation of the median lethal dose LD50 of one of the prepared Nitrone compound B1 on laboratory rats , the result was that the prepared compound was non toxic at the used doses ( 34.2-136.8 ) . | We also study the biological activity of the prepared compounds ( Alaldehydes and Nitrones ) by observing its effect on negative and positive bacteria of gram dye

دراسة وظائف الكبد وصورة الدهون والاجهاد التاكسدي في مصول النساء قبل وبعد استئصال المرارة في محافظة ذي قار / العراق == Study of Liver Function, Lipid Profile and Oxidative Stress in Sera of Women Pre and Post Cholecystectomy in Province of Thi - Qar/ Iraq

Author name: سمى يعقوب يوسف
Supervisor name: رائد معلك الصالح | مهند عبد الرضا الشريفي
General topic: Chemistry
Specific topic: Analytical Biochemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: English
University location: Dhi Qar
Abstract: The present study has been designed to evaluate and compare changes in patients pre, post and long periods for cholecystectomy on BMI, liver function (Aspartate Amino Transferase (AST), Alanine Amino Transferase (ALT), Alkaline Phosphatase (ALP), Total Bilirubin (TSB), Total Protein (TP), lipid profile (Total Cholesterol (TC), Triglyceride (TG), High Density Lipoprotein (HDL), Low Density Lipoprotein (LDL), Very Low Density Lipoprotein (VLDL)), oxidative stress (Malondialdehyde (MDA), Nitric Oxide (NO)) and antioxidant state (Albumin (Alb), Ceruloplasmin (CP)). | The study includes (192) subjects : (64) normal subjects (control) and (128) patient’s cholecystectomy, their age range (20-69) years, the patients were divided in to three groups : (64) patients pre and 24 hr post operation cholecystectomy, (64) patients after long periods for cholecystectomy, as well as the patients were divided by age into two groups : a premenopausal group and a postmenopausal group. | The results show that there were a significant decreased in the concentration of serum (AST, ALT, TSB, DB, InB, HDL and Alb) in group pre in comparison with each of post (short and long terms) and control groups (p≤0.05). It was found no significant differences in the concentration of serum (AST, ALT, TSB, DB, InB, HDL and Alb) between each of post (short and long terms) groups (p≤0.05). Also it was found significant differences in the concentration of serum (AST, ALT, TSB, DB, InB, HDL and Alb) between each of post (short and long terms) and control groups (p≤0.05). | -----------------------------INDEX--------------------------------- | XII | While the results showed a significant increase in the concentration of serum (ALP, TP, TC, LDL, NO, MDA and Cp) in all patient groups in comparison with control groups (p≤0.05). It was found no significant differences in the concentration of serum (ALP, TP, TC, LDL, NO, MDA and Cp) between each of post (short and long terms) groups (p≤0.05). Also it was found significant differences in the concentration of serum (ALP, TP, TC, LDL, NO, MDA and Cp) between each of post (short and long terms) and control groups (p≤0.05). | Also the results showed a significant increase in the concentration of serum TG and VLDL in all patient groups in comparison with control groups (p≤0.05). It was found no significant differences in the concentration of serum TG and VLDL between each of post (short and long terms) groups in the group A (p≤0.05). But it was found a significant difference in the concentration of serum TG and VLDL between each of post (short and long terms) in the group B (p≤0.05). Also it was found a significant difference in the concentration of serum TG and VLDL between each of post (short and long terms) groups and control groups (p≤0.05). | The correlation between nitric oxide and each of (ALP, TP, TC, TG, LDL, VLDL, MDA and Cp) in these patient groups were positive. Whereas the correlation between nitric oxide and each of (AST, ALT, TSB, BD, InB, HDL and Alb) in these patient groups were negative. | The above reviewed results lead to conclusion that cholecystectomy causes variant alternations in serum hepatic function and lipid profiles and causes variant effects in serum oxidative stress. Also, age has no effect on each of (ALT, TSB, DB, InB, ALP, TP, TG, VLDL, NO, MDA, Cp and Alb), while age has effect on each of (TC, LDL and HDL). Besides, there are no effect of the period after cholecystectomy on all studied parameters except TG and VLDL.

تحوير فجوة طاقة ثاني اوكسيد التيتانيوم بواسطة تفاعلات الحالة الصلبة مع صوديوم بوروهيدريد والمنيوم ليثيوم هيدريد وتحديد فعالية التحفيز الضوئي == Modifying The Band Gap of Nano Titanium Dioxide By Solid State Reactions With Aluminum Lithium Hydride and Sodium Borohydride and Determining Their Photocatalytic Activity

Author name: سراج علي رحيم
Supervisor name: محسن عريبي الدخيلي | ابراهيم عبود فليفل
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: English
University location: Dhi Qar
Abstract: This study includes preparation of nanoparticles of titanium dioxide using sol-gel method and then, the band gap was modified by solid state reaction with (AlLiH4،NaBH4) reductive compounds. Modification reduced the band gap separating | energy levels between valance band (VB) and conduction band (CB), therefor; facilitating the transfer of excited electrons from (VB) to (CB). Absorption of the energy from incident photons having the same or larger energy than the energy of the | band gap promote the formation of the couple (electron - hole) . The resulting (e--h+) couple acts to produce (OH.) radicals. OH. radicals hav a high capability to destroy organic pollutants that adsorbed on surface of the photocatalytic TiO2. | The optical properties measured using UV-visible spectrophotometer (Absorbance (A), energy band gap (Eg) and absorption coefficient ( α ) . TiO2 and TiO2- solid state reaction showed clear blue shift of the absorption band gap which were (2.8ev, 2.7ev, 2.25ev, 2.0ev) to )TiO2- NaBH4(550 ) ,TiO2-NaBH4 (750 ) , TiO2-AlLiH4 (500 ) and TiO2 -AlLiH4 (750 )) respectively. The structure of prepared TiO2 nanopowders were identified using XRD, particle size distribution varied appreciably in comparison with crystallite size (D) calculated from Sheerer formula which was in a good accordant compared with ASTM results , the particle size and their distribution were characterized using (AFM) . To the surface forms and compositions diameters of nanoparticles)SEM) was implemented . The energy dispersive X-ray (EDX) microanalysis was utilized to investigate the chemical composition of the whole samples. | Photocatalytic reaction was studied by using UV-Vis spectrophotometry. | In photocatalytic reaction the effect of the catalyst on photocatalytic rate of decomposition of methylene blue dye through the use of catalyst TiO2 and TiO2- solid state reaction (TiO2 - NaBH4 (550 ,750 )) and (TiO2 - AlLiH4 (500 ,750 )) . Using constant weight of the catalyst and dye. The most effective weight was found (1*10-4 M). At best weight the influence of many factors on rate of decomposition of dye were studied the impact of change pH varies (4.5, 7.1 and 9.4) found that the highest percentage in the decomposition of the MB was in the acidic media than in neutral and then alkaline. The effect of temperature variation from (20, 30, 40ºC) and found that increased rate of decomposition with increasing the temperature of the MB. Activation energy (Ea) for each reaction was calculated by using the equation of Arrhenius equation between (5.73-11.31) kJ mol-1 . | A series of dark reactions with absorbance measurement by UV-Vis spectrophotometry, within different periods of time with the change of pH and temperature. The results indicate that no degradation of the methylene blue dye although all the factors affecting in photocatalytic present except UV-light .

التحقيق في اثار الحجامة الرطبة على بعض المؤشرات البايوكيميائيه في ذي قار محافظة / العراق == Investigation of The Effects of Wet Cupping Therapy on Some Biochemical Parameters in Thi - Qar Governorate/ Iraq

Author name: زهراء طالب مشلول
Supervisor name: محمد عجة عودة
General topic: Chemistry
Specific topic: Analytical Biochemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: English
University location: Dhi Qar
Abstract: This study was designed to determine the effect of cupping to treat or reduce a lot of blood variables such as diabetes, liver failure, lipid profile and status of Oxidative and antioxidant , where we have in this study to take blood samples from the volunteers before they activate cupping therapy and then we have to take more samples within 14 days and comparing the results obtained were as follows : The results of the blood glucose concentration decreased significantly (P≤0.05) post cupping when compared with a pre-cupping, while there is no significant decrease in the level of glucose in the blood serum of a group post cupping compared with the control group (P≥0.05 ). In addition, the group pre-cupping showed a significant increase (P≤0.05) in the glucose in the blood serum when compared with the two sets of post-cupping and the control group. It can be seen the results of MDA serum showed a decrease (P≤0.05) in the group post cupping, compared with a pre-cupping, while non-significant in the serum level of MDA in the group post cupping compared with the control group (P≥0.05). While the group pre cupping significant (P≤0.05) MDA in serum when compared with the two sets of post-cupping and control. Summary | XIV | Cp serum levels showed high significant increase (P≤0.05) in | serum Cp can be observed in the two groups pre and post cupping when comparing this with the control group, In addition, the total post-cupping has shown a significant decrease (P≤0.05) in serum Cp compared with a pre-cupping. | As well as the results showed Alb serum significantly increased (P≤0.05) in Alb serum can be observed in the two groups pre and post cupping when compared with the control group, as a group post the cupping showed that there was a significant decrease | (P≤0.05) in Alb serum compared with a pre cupping. | Liver function tests showed a significant decrease in the group post cupping, compared with a pre cupping (P≤0.05), while significant difference was observed liver enzymes levels (ALT, ALP and AST) in the serum can be observed in a post-cupping compared with the control group (P≤0.05). Moreover, the group pre-cupping showed a significant increase (P≤0.05) in levels of ALT, ALP, AST serum when the two groups to be compared with the postcupping and the control group. | Fat results in the serum showed little change, but did not reach the moral (P≥0.05) in the proportion of fat in the blood serum levels of lipoproteins among all groups studied. | In the end we can say that cupping is not used for treatment once and for all, but it's used to treat Alternatively, or in a more identification used to treat complementary.

طريقة كروماتوغرافية طيفية جديدة - لتقدير عقار اللوراتادين في بعض المستحضرات الصيدلانية == Anew Chromatographic - Spectrophotometric Method for Determination of Loratadine in Some Pharmaceutical Preparations

Author name: صفاء حكيم ناصر الغزاوي
Supervisor name: محمد تركي خثي
General topic: Chemistry
Specific topic: Analytical Biochemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: English
University location: Dhi Qar
Abstract: Due to the medicinal significance of Loratadine, ethyl4-dihydro-11H benzo [5,6] cyclohepta [1,2-b] pyridin-11ylidene (-1-piperidinecarboxylate) has been devoted to this message To create a new chromatographic-spectral method for estimating the pure drug and the drug found in a number of its pharmaceuticals. | The letter included a detailed explanation of a new chromatographic-spectral method for estimating amounts of pure and commercial loratidine. The principle of this method is to break down the double bond present in the loratadine by the potassium permanganate oxidant factor of 0.05 molar and convert it into two ketone-containing compounds : 8-Chloro-5,6-dihydro-11H-benzo [5,6] cyclohepta [1,2-b The second compound is ethyl-4-oxopiperidine-1-carboxylate (B). It has been shown that the two compounds (A and B) can be separated by TLC, FTIR, separated and completely isolated by column chromatography technique. After the separation, the compound (A) was given a stable colorant complex with 4-amino acid benzoic acid ester, in a acidic medium, While the compound ( B ) did not give a stable complex. The results showed a study of changing the conditions of the process of analysis and separation of the two compounds and their diagnosis and the formation of the resulting complex and applications of the method and discussed with the use of different quantities of many types of acids and strong and weak rules and indicate their impact on the intensity of the complex complex color and the optimal conditions were selected for his way of work.

تخليق وتشخيص لبعض المركبات الحلقيه الغير متجانسه كالبيتا لاكتام والكاما لاكتام وفق تفاعل كانيكوزا == SYNTHESIS AND CHARACTRIZAITION OF SOME NEW HETROCYCLIC COMPOUNDS INCLUDING ? & ? LACTAMS BY USING KINUGASA REACTION

Author name: دعاء هادي محسن العطار
Supervisor name: محمود شاكر مكطوف | محسن عريبي الدخيلي
General topic: Chemistry
Specific topic: Organic Chemistry
Degree: Master
University: University of Thi-Qar - College Of Science - Chemistry Department
Language: English
University location: Dhi Qar
First pages:
Abstract: This study is concerned with the synthesis and characterization of the some β- lactams 3(a-f),as in (Table.2). These compounds 3(a-f) were prepared by reacting phenylactylene with the appropriate nitrones2(a-f), in the presence of triethylamine | in acetronitrel under nitrogen atmosphere at -10˚C. in moderate yield (50-70)% . The nitrones compound 2(a-f) were prepared by reacting aldehyde with appropriate N-phenyl hydroxyl amine 1 in the presence of Ethanol. | As in (Table.1) Also the N-phenyl hydroxyl amine 1 compounds were prepared by reduction of nitrobenzene with ammonium chloride in Zinc Powder in the presence of water.This study is concerned with the synthesis and characterization of mono-γ- | lactams and bis-γ-lactams These compounds were prepared by reaction phenylsuccinic anhydride with the appropriate schiff bases(imines), by using chloroform solvent and heated at temperature (51-61˚C) in moderate yields(70- 92)%, All this compound confirmed by using spectra data such as : , IR , 1H-NMR , 13CNMR , APT 13C-NMR , HSQC 1H-13C-NMR,Mass

عدوى المسالك التناسلية الخارجيه بين النساء مرتبطة مع بعض الهرمونات في محافظة ذي قار العراث == External genital tract infections among women association with some hormones in Thi - Qar provice - Iraq

Author name: صفا عبد الوهاب وجيه اليعقوبي
Supervisor name: باسم عبد الحسين | مهند عبد الرزاق
General topic: Biology
Specific topic: Microbiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

التغيرات الموسمية لبعض العناصر الثقيلة والبكتيرية في الحماة المستجمعة من محطة معالجة المياه العادمة في مركز مدينة الناصرية - العراق == Seasonal variation of some heavy elements and bacterial in the sludge collected from the wastewater treatment plant in the center of Al - Nasiriyah city, Iraq

Author name: نورالدین صباح ناهي
Supervisor name: باسم یوسف الخفاجي | سعد سلمان ھمیم
General topic: Biology
Specific topic: Environment - Environmental pollution
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: Arabic
University location: Dhi Qar
First pages:

دراسة مصلية وجزيئية لبكتريا اللولبيه البوابية في الاشخاص المصابين بمشاكل المعدة ومنها سرطان المعدة == Serological and Molecular Study of Helicobacter pylori in Gastric Problem Patients Including Gastric Cancer

Author name: بيداء مزهر كاظم
Supervisor name: منال بادي صالح
General topic: Biology
Specific topic: Microbiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

عزل وتحديد بعض الصفات الجزيئية لبكتريا Streptococcus mutans من مرضى تسوس الاسنان والصفيحة السنية في محافظة ذي قار /العراق == Isolation and Detection of Some Molecular Characterization of Streptococcus mutans from Dental Caries and Dental Biofilm patients at Thi - Qar Province/Iraq

Author name: حمزة شاكر عبد الزهرة
Supervisor name: منال بادي صالح
General topic: Biology
Specific topic: Microbiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

تاثير المركبات الفينولية المستخلصة من نباتي اوراق اكليل الجبل Rosmarinus officinalis وبذور العنب Vitis vinifera في اناث الجرذان المختبرية عالية الكولسترول == Effect of Polyphenolic compounds extracted from Rosemary leaves (Rosmarinus officinalis) and Grape seeds (Vitis vinifera) on hypercholsterolemic female rats (Rattus norvegicus)

Author name: يقين ريسان شعلان
Supervisor name: خالد الفرطوسي
General topic: Biology
Specific topic: Zoology - Physiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

تاثير انبعاثات محطة الطاقة الحرارية في تراكيز بعض العناصر الثقيلة و بعض المحتويات الكيموحيوية لنوعين من النباتات البرية الحمض Suaeda vermiculata و العاقول Alhagi maurorum في مدينة الناصرية - جنوب العراق == Effect of thermal power station emissions on the concentration of some heavy elements in soil and two species of wild plants (Alhagi maurorum and Suaeda vermiculata) in Al - Nasiriyah city/ south of Iraq

Author name: هدي ناطق فارس الخفاجي
Supervisor name: حيدر راضي مالح | باسم يوسف الخفاجي
General topic: Biology
Specific topic: Life Science
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: Arabic
University location: Dhi Qar
First pages:

تاثير المركبات الفينولية المستخلصة من نباتي الكركم Curcuma longa والبروكلي Brassica oleracea var italic في بعض المعايير الفسلجية لذكور الجرذان المختبرية norvegicus Rattus المصابة تجريبيا بالتهاب المفاصل == Effect' of phenolic 'compounds extracted from Curcuma longa and Brassica oleracea var italic on some physiological parameters of male rats (Rattus : norvegicus) affected with induced arthritis

Author name: منى كريم فهد
Supervisor name: خالد كاطع وشيل الفرطوسي
General topic: Biology
Specific topic: Life Science
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: Arabic
University location: Dhi Qar
First pages:

الكشف المظهري والجيني عن البكتريا السالبه لصبغة كرام المقاومه للمضادات الحياتيه المعزوله من النساء الحوامل المصابات بالتهابات المسالك البوليه في محافظة ذي قار == Phenotypic and Genotypic Detection of Antibiotics Resistant Gram Negative Bacteria Isolated from Urinary Tract Infection among Pregnancy Women in Thi - Qar Province

Author name: ناصر صالح لهواك
Supervisor name: يحيى عبد الرضا عباس
General topic: Biology
Specific topic: Microbiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

الصفات الجزيئية وتكوين الاغشية الحيوية للمكورات العنقودية والزوائف الزنجارية المعزولة من الاصابات الجلدية == Molecular Profile and Biofilm Formation of Staphylococcus aureus and Pseudomonas aeruginosa Isolated from Skin Infections

Author name: انتصار عامر هاشم
Supervisor name: قاسم حسن وداعه | احمد خصاف عطيه
General topic: Biology
Specific topic: Microbiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

عزل والتوصيف لجزيئي لبكتريا Vibrio. Fluvialis من الاطفال المصابين بالاسهال في محافظة ذي قار == Molecular Characterization of Vibrio. fluvialis from Diarrheal Children in Thi - Qar province

Author name: حوراء احمد محمد
Supervisor name: عزت حسين مزعل
General topic: Biology
Specific topic: Microbiology
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

دراسة مناعية كيمونسجية للتعبير عن بروتين الايلاستين بين النساء العراقيات المريضات بسرطان الثدي في محافظة ذي قار == Immunohistological Study of Elastin Protein Expression Among Iraqi Women Patients with Breast Carcinoma at Thi - Qar Province

Author name: لمياء علي كاظم السعداوي
Supervisor name: هيفاء عبد علي الشمري
General topic: Biology
Specific topic: Life Science
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

كفاءة الموجات الدقيقة Microwaves في السيطرة على حشرة عثة التمر Lepidoptera : Pyralidae) Ephestia cautella Walker) ودورها في تقليل التلوث بالفطريات المصاحب للاصابة بها == Microwaves efficiency in controlling the insect of the date moth Ephestia cautella (Walker) (Lepidoptera : Pyralidae) and its role in reducing the contamination of fungi associated with infection

Author name: احسان حميد خضير
Supervisor name: صادق ثاجب علي
General topic: Biology
Specific topic: Life Science
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: English
University location: Dhi Qar
First pages:

التشخص والشجرة التطورية لفيورس كمسبب رئيس لالتهاب المعدة والامعاءفي الاطفال في محافظة ذي قار == Detection and phylogentic Tree of Norovirus As a Main Cause for Gastroenteritis among Children at Thi - Qar Province

Author name: دعاء كامل محمد الموسوي
Supervisor name: رحمن لعيبي جلاب الركابي | باسم عبد الحسين جار الله
General topic: Biology
Specific topic: Microbiology - Viruses
Degree: Master
University: University of Thi-Qar - College Of Science - Department Of Biology
Language: Arabic
University location: Dhi Qar
First pages:
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