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تحضير وتشخيص ودراسة الفعالية البايوكيميائية لبعض مشتقات ? لاكتام
اسم المؤلف:
عذراء محمد علي
اسم المشرف:
علي هاشم عيسى | سميرة احمد زيارة
الموضوع العام:
علوم الكيمياء
السنة:
2017
الموضوع الدقيق:
الكيمياء
الدرجة:
ماجستير
الجامعة:
جامعة البصرة - كلية العلوم - قسم الكيمياء
اللغة:
العربية
مكان الجامعة:
البصرة
الصفحات الاولى:
المستخلص:
The Staudinger reaction of imines to β - lactams was successfully achieved using chloroacetyl chloride and tertiary amines in dry toluene under mild conditions. Two new types of β - lactams have been synthesized by this versatile and efficient method in good to excellent yields.R2 R1 الرمز Br NO2 A CN NO2 M OCH3 OCH3 F Br OCH3 B The imines were synthesized according to the literature procedure by reaction of substituted aldehydes and substituted anilines.The chloroacetyl chloride has been synthesized by the reaction of chloroacetic acid with phosphorus pentachloride (PCl5) and used directly with out any purifications.All products were characterized using IR, H and C NMR. This method is simple, clean, and the by - products were removed by simple aqueous work - up. The effects of solvents, molar ratio of reagent, and the temperature were considered.The antibacterial acttivity of the compounds A, M and F has been studied on gram positive isolates (Staphylococcus aureus and Bacillus) and gram Negative isolates (E. coli and Psedomonas), in comparison with standard antibiotics which are : Ampicillin, Amoxicillin and Cephalexin.The results showed the influence of the effectiveness of inhibitory compounds on all bacterial isolates at concentration (250 mg / ml). The study also included the estimation of minimum inhibition concentration of these compounds at all examined bacterial isolates. The results showed the contentiously effectiveness of the compounds (A, M) in the inhibition of the gram positive Staphylococcus aureus spp. up to focus (25 μg / ml). In addition, our study includes determination of the effect of compounds A, M and F on human fresh red blood cells as cytotoxicity in concentrations (1,5,25,50,250 mg / ml). The results were revealed that there was non - hemolysis of red blood cells, so it can be considered these compounds are non - toxic on the human red blood cells.The effect of studied compounds (A, M, F) at concentrations (50, 125, 250 mg / ml) dissolved in DMSO solution, were determined to detect the symptoms of hypersensitivity test using the domestic rabbits, no appearance of any symptoms were observed for hypersensitivity Lalani swelling and redness, or itching after injection of these compounds for the first time, as well as after the exposure to these compounds after Done week measure, the level of antibodies type lgE and white blood cells type acidic Eosinophil, were measured after injection of these compounds which not get any significan
👁 مشاهدة
اداة تقييم الخطر لتنبؤ احتمالية الاصابة بسرطان الثدي بالاستناد على عوامل الخطر الديموغرافية واستخدام خوارزمية الشبكة العصبية الضبابية == Risk Assessment Tool - based Demographic Risk Factors to Predict Probability of Breast Cancer accident using Neuro - fuzzy Technique
اسم المؤلف:
دنيا سمير مزهر
اسم المشرف:
كريم راضي حسن
الموضوع العام:
علوم الحاسبات
السنة:
2017
الموضوع الدقيق:
علوم الحاسبات
الدرجة:
ماجستير
الجامعة:
جامعة البصرة - كلية العلوم
اللغة:
العربية
مكان الجامعة:
البصرة
الصفحات الاولى:
المستخلص:
In recent years, the statistics presented high incidence rates of breast cancer.So, early detection of breast cancer considered one of the highest healing rates for most cases, where the treatment at early stage is very easy and involves removal to malignant tumor from breast without needed to remove all breast. As well the cost of treatment is very economical with early diagnosis, while at a late stage, the cost associated with treatment is higher. In addition, the prevention have role to reduce risk by avoid catalysts that cause Incidence and associated with risk factors. For these reasons and others, we present the proposed method for designing a risk assessment tool for breast cancer prevention and early detection based on demographic risk factors (DRF) and using Neuro - Fuzzy System (NFS) in designs risk assessment model that help doctors and patients in assess risk of Incidence through providing better and more reliability results.In this thesis, the proposed method is a process of several stages. The first phase included statistical study to identify problem of research based on statistics in Basra, through apply the study on patients community at Al - Sadir Teaching Hospital in Basra (Oncology Center), that represent main center in Basra for the treatment of cancer. Three and most important phase includes the proposed approach for design assessment model using Neuro - Fuzzy system (NFS) in two approaches. the second approach suggested using Fuzzy c - means (FCM) algorithm with Neuro - Fuzzy system to improve the first approach that just use Neuro - Fuzzy system (NF). The proposed method is focused to solving basic research problem to prevention and early detection of breast cancer.The proposed method achieved high results when compared to other methods and tools. The success rate of proposed assessment tool is 94%, and it is higher rate among other assessment tools (Gail, IBIS) that obtained by match the result for assessment of test data (50) with the expert opinion (the real result). Programming and testing of proposed method by used Matlab 2013
👁 مشاهدة
اخفاء معلومات في ملف صوتي باستخدام تقنيات التشفير الانسيابي والمواقع العشوائية
اسم المؤلف:
اسماء عزيز جابر
اسم المشرف:
حميد عبد الكريم يونس
الموضوع العام:
علوم الحاسبات
السنة:
2017
الموضوع الدقيق:
علوم الحاسبات
الدرجة:
ماجستير
الجامعة:
جامعة البصرة - كلية العلوم
اللغة:
العربية
مكان الجامعة:
البصرة
الصفحات الاولى:
المستخلص:
The rapid development and tremendous computer and communication technologies and the proliferation of global networks, has led to the emergence of many techniques to transfer confidential information including encryption (Cryptography), and as a result of piracy And penetrating these techniques need arose for techniques and methods more sophisticated and difficult to transfer confidential information securely. Because of the increase in the number of attacks recorded during the exchange of electronic information between the source and the recipient may need to use a more powerful way to secure data transfer, encryption methods are combined And hide the information together for the purpose of setting up a mechanism to improve confidentiality and because these methods shared goals and common services in protecting the confidentiality, integrity and availability of information from unauthorized access and thus check mechanism High security integration to preserve data confidentiality.The research aims to use the method to hide secret information (picture or sound) into audio files (audio file) (wav) as cover in such a way as to ensure that information is not piracy, secret message encryption Sleek encryption before concealment by making the size of the stego - audio is equal to the size of the original file.As the audio file is the output of a process of hiddin similar to the original file and for the human ear to feel the change. By segmenting the original soundtrack cover frames (frames) and apply the random function to locate hidden after the colored image layers in case confidential information picture or sound to hide the hash to Frameworks and then applying the function for selecting locations for concealment and then apply the least significant bit technology (Siginfcant Least Bit) for concealment.In the case of the recovery process is contrary, embedded audio file fragmentation occurs (stego - audio) and apply the random function for selecting locations for concealment and decrypt the message.Use a key in a hash process sound represents the size of the picture you want to hide, and it represents the number of frames (frames) and serve as a key to encrypt the original audio as we use an algorithm to generate a sequence of key Homologous between the sender and recipient to Sleek encryption to increase security. The recovery process success ratio for the image dB 99.0, audio retrieval process was well proportioned. , We used Image metrics (PSNR), (SNR) and the inclusion ratio between the confidential letter and sound and cover (RMSE) between audio - stego and original sound. And high results were obtained about (85 - 95 )when recovery without any mention on the file (Stego_audio).
👁 مشاهدة
عنقدة النصوص العربية باستعمال تحليل الاحالة المشتركة == Arabic Text Clustering Using Coreferance Resolution
اسم المؤلف:
فراس حمودي نعمة
اسم المشرف:
سلمى عبد الباقي محمود
الموضوع العام:
علوم الحاسبات
السنة:
2017
الموضوع الدقيق:
علوم الحاسبات
الدرجة:
ماجستير
الجامعة:
جامعة البصرة - كلية العلوم
اللغة:
العربية
مكان الجامعة:
البصرة
الصفحات الاولى:
المستخلص:
Clustering texts organizes texts in subsets coherent and internally consistent, and different with each other. These subsets called clusters. The documents combines according to the similarity measures, that rely on features extracted of the documents. This technique applies in various fields such as web mining, search engines, and information retrieval. Clustering documents gives information retrieval, automatic extraction, and representation efficiently without user intervention for increasing growth of the new documents.This study aims to improve the accuracy and efficiency of arabic texts clustering. To achieve the aim of this study two approaches are used. The first approach uses the standard technique in Arabic texts clustering. The second approach is proposal to reduce features of the texts.The first approach is applied (K - medoids, K - means) and similarity measures (Euclidean, cosine). The problem of this approach is that huge of the features, which influence the efficiency and coherence of the clusters.The huge features for the documents adds challenge and lead to high dimension so coreference resolution technique approach is applied. This technique extracts main subjects for each document to improve arabic documents clustering in order to achieve the goal of our study. The system implements using a corpus contains on 200 sport news Arabic.Finally, evaluation measures are used including (Precision, Recall and F - measure) to evaluate our system, and we obtain acceptable results.First method exceed K - medoids and using similarity measures (Euclidean, Cosine) where highest values (0.60, 0.78, 0.67) of the method of k - means. In addition, the results of the proposed second way exceeds method of K - medoids and using similarity measures (Euclidean, Cosine) with coreference resolution, where the measures values (0.80, 0.83, 0.81).
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