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تحضير ودراسة بايلوجية لبعض مركبات البايرزول == Preparation and biological study of some pyrazole compounds
اسم المؤلف:
خنساء صقر سعود
اسم المشرف:
نزار لطيف شهاب الدين
الموضوع العام:
علوم الكيمياء
السنة:
2015
الموضوع الدقيق:
الكيمياء
الدرجة:
ماجستير
الجامعة:
جامعة البصرة - كلية التربية للعلوم الصرفة - قسم الكيمياء
اللغة:
العربية
مكان الجامعة:
البصرة
الصفحات الاولى:
📎 25T1582 - p.pdf
المستخلص:
The present study includes the preparation of some pyrazolines derivatives includes their characterization and their biological activity.Chapter one the introduction shows the literature survey and related important reactions for pyrazolines .While chapter two shows the details of the preparation for each types in details 36 pyrazoline product were prepared from 6 types of (cha/cones) Benzalacetophenones and six different hydrazine ( hydrazinehydrate , phenylhydrazine, semicarbazide, thiosemicarbazide 2,4 - dinitrophenylhydrazine and phenylthiosemocarbazide ).Chapter three shows all the results which proved the chemical structures of some selected compounds by using I.R, 1H - NMR, 13C - NMR, CHN, and mass. Spectroscopy we found abnormal case in pyrazoline derivatives especially in the ring once have - CH2 like in (P1and P10) and compounds (P8 and P13) does not have the methylene protons this exception was happened due to modification in procedure. Finally the biological activity for some selected compounds were used and compared with standard drugs and its shows moderately to good activity.
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