استخدام هيدروكلوريك ثلاثي فلوبيرازين (TRF) ككاشف عضوي في التحليل الطيفي لبعض المستحضرات الصيدلانية == Utilizing of Trifluoperazine Hydrochloride as an Organic Reagent in the Spectrophotometric Analysis of some Pharmaceuticals

Author name: رضوان جواد ضاحي
Supervisor name: مهيمن محمد مجيد الرفيعي
General topic: Chemistry
Specific topic: Chemistry
Degree: Master
University: University of Kerbala - College Of Science - Chemistry Department
Language: English
University location: Karbala
Key words:
  • 1-6 Trifluoperazine Hydrochloride (TRF)
  • 1-7 Spectrophotometric Methods of Analysis 13
  • 1-8 Types of Reactions in Spectrophotometry
  • 1-8-1 Diazotization-Coupling Reaction 13
  • 1-8-2 Pharmaceutical Analysis of Chromogenic Interactions
  • 1-9 Analytical Methods used for the Determination of the Drugs Studied
  • 1-9-1 Methods of Analysis for the Determination of (MCP)
  • 1-9-2 Methods of Analysis for Determination (MTZ)
  • 1-9-3 Methods of Analysis for the Determination of (CAP)
  • 2-5-2-2 Reduction of nitro group to amine Error! Bookmark not defined.
  • 2-5-2-3 Standard Solution of MTZ 500 µg.ml-1 Error! Bookmark not defined.
  • 2-5-2-4 Trifluoperazine hydrochloride (TRF) reagent 1.5x10-2M 36
  • 2-5-2-5 Sodium persulfate 4x10-3M
  • 2-6 Optimization of parameters in experimental
  • 2-6-1 Determination of absorbance and composition of the colored product 38
  • 2-8-2 Construct a Calibration Curve with an MTZ Drug 41
  • 2-8-3 Construct a Calibration Curve with a CAP Drug
  • 2-9 Research the Nature of Soluble Colorful Products
  • 2-10-3 Chloramphenicol Pharmaceutical Preparations Solution 45
  • 2-10-3-1 Method for Drops
  • 2-11 Solutions Created to Research the Drug's Analytical Uses on (Serum) 45
  • 3-1-2-4 Addition Sequence Effect 51
  • 3-1-2-5 The Stability of the Colored Product 52
  • 3-1-2-6 Temperature's Impact on Colored Products 53
  • 3-2-2 Optimal Conditions for the Reaction 66
  • 3-2-2-1 The Effect of the Type of Acid Used
  • 3-2-2-2 The Effect of the volume of the Reagent TRF Used 67
  • 3-2-2-3 The Effect of the Oxidizing Agent on the Reaction
  • 3-3-2-1 The Effect of the Type of Acid Used
  • 3-3-2-2 The Effect of the volume of the Reagent TRF Used
  • 3-3-2-3 The Effect of the Oxidizing Agent on the Reaction
  • 3-3-2-4 Addition Sequence Effect
  • 3-3-2-5 The Stability of the Colored Product 86
  • 3-3-2-6 Temperature's Impact on Colored Products
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